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GCMS analysis results for sample AE11602, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013943–000013967

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) *= Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclopentane, 1,1-dimethyl- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 10.31 0.50 ug/1 31951 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentane, 1,1-dimethyl- 98 C7H14 001638-26-2 42 2 Cyclobutane, 1,2-diethyl-, trans- 112 C8H16 019341-98-1 38 3 Cyclobutane, 1,2-diethyl-, cis- 112 C8H16 061141-50-2 33 4 1-Pen 3,4-dimethyl- 98 C7H14 007385-78-6 33 Abundance Scan 575 (10.313 min): 11602.D (-) m/z 56.10 100.00% 56 43 5000 69

83 -A— 10.00 10.20 10.40 10.60 -rrpTTTp-rTTpTTTp-n+j- 4.51 mHmmAMHH m/z 55.10 75.25%

A mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #1333: Cyclopentane, 1,1-dimethyl- 56 41 69 5000 83 A TdT 10.00 10.20 10.40 10.60 27 m/z 43.05 61.92% ,j,.... j.......98

jA_ l““l npph TTTH i.(।(j.... ।, n/z-> 20 25 3035404550556065 70 75 80859095 100105110115120 Abundance #2701: Cyclobutane, 1,2-diethyl-, trans- 41 55 T ‘ I ' ‘ ‘ ' I ' ' ‘ ' I 10.00 10.20 10.40 10.60 5000 m/z 41.15 53.22% 27 70 84

rnfe-> Abundance mpmrll ’ ’ I’’ l 112 > |. >. .| .< .. |■ 1I >| II I l|■ l ■> [I II Il ! 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 .. /Uy #2733: Cyclobutane, 1,2-diethyl-, cis-

. . AN 4(1 55 10.00 10.20 10.40 10.60 m/z 69.10 42.61% 5000 27 70 84 , 1 112 ।. 1.11....j,11 i11111(I[>j....j, 111,j i। > ri»j. j i > j 11 n । > i n ।, ‘ ' I ‘ ‘ ‘ I • ' ' ‘ I ' 1 ' ‘ I ' ' ' ' I /z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 10.00 10.20 10.40 10.60

11602.D GCMS0520.M Fri May 24 08:33:09 2002 Page 5

NYC-WTC_000013952

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