GCMS calibration table for method GCMS0412, April 2002

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Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

NYC-WTC_000047701–000047714

Folder label: “GCMS X 4/4/02 A 4/12/02”

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Data File : C:\HPCHEM\1\DATA\APR1102\8 016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hexanal Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

7.18 0.41 ug/1 50024 1,4-Dichlorobenzene-d4 12.23

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal / 100 C6H120 000066-25-1 78 2 Cyclobutanol , 2-ethyl- 100 C6H120 035301-43-0 36 3 3 -Buten-1-ol , 2-methyl- 86 C5H10O 004516-90-9 12 4 Pentane, 4,2,4-trimethyl-________ 114 C8H18 000540-84-1 9 Abundance Scan 232 (7.175 min): 8016.D (-) m/z 43.95 100.00% 44 56

5000 39 72 82 67 6.80 7.00 7.20 7.40 7.60

m/z-> i" ■ ■ ।। ■11 11111'11 +49— • I' ■ 11 — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 56.00 88.68% Abundance #1573: Hexanal ________________ _____ 44 56

5000 I I I II ( I I I I t I I I I I I 1 I I [ I

27 680 7.00 7.20 7.40 7.60 72 m/z 41.05 77.21% 67 82 I - “100030003093"0 100 ——0T—01T1Tr " ' i11111 '1111111 ■ '1 r 1" i " " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000 44 #1521: Cyclobutanol, 2-ethyl- 57

72 M 1 । ■ 1 ■ 1 1 1 1 1 1 1 1 1 ' ■ । 6.80 m/z 7.00 57.00 7.20 7.40 67.14% ' 1 1 ' 7.60 27

53 67 82 r" 'i i" " i i I - —mp— 11" 11 ■1" 1 TTI > i1" ' 1111' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #695: 3-Buten-1-ol, 2-methyl- 56 1 AaN A...... ' Ut ' ' I 1 ■ ■ ' i ■ 11 । । । > । । । । 680 7.00 7.20 7.40 7.60 m/z 43.05 56.63%

5000 31 39

n/z-> " 1111' 11 TH ■' i11 50 I' ‘11 r " ■ I ‘' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 .... 68 ||, 1....... 86........... 11" " r 11' 11" ' 1" ' ‘ r " ' r " 1TTTI ’ ’’I’II’I’I AM 6.80 7.00 7.20 W ' 1 I r 1 ' 1 | 1 7.40 Aa 7.60

8016.D GCMS0412.M Tue Apr 16 12:08:04 2002 Page 1

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