Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
NYC-WTC_000046249–000046265Folder label: “GCMS X 5/7/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C: \HPCHEM\1\DATA\MAY0302\9579.D Vial: 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 Hexanal Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 7.13 3.26 ug/1 198881 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexanal 100 C6H120 000066-25-1/90 2 Cyclobutanol, 2-ethyl- 100 C6H120 035301-43-0560 3 Butanal, 3-methyl- 86 C5H10O 000590-86-3 28 4 Oxirane, 2-methyl-3-(1-methylethyl) 100 C6H120 001192-31-0 12 Abundance Scan 228 (7.131 min): 9579. D (-) m/z 44.05 100.00% 44 56 A 5000 39 ____________ 72 —1 r | ’ 1 । | I i i r j i i i'"I"|" I I I । 1[ “ I
67 82 6.80 7.00 7.20 7.40 51 111111111J11-11 A - ......................................... i1" ‘ r " ' i T -+H [>" 1 | " ‘rpv i I | I > i i | i i > i | i i m/z 56.10 72.25% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1573: Hexanal 44 56
5000- 1 1 ' I r 1 1 ' I 1 ' r l-l ' ' 1 1 I1 1 1 ' I 27 6.80 7.00 7.20 7.40 72 m/z 41.05 72.08% 67 82 । I | I I I I , j I I j ! I | I I | 100 i11'11 | i | I I I I | I I I > | I I r I । < i i i । i i i i । । । 11111111111 111" 111 mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1521: Cyclobutanol, 2-ethyl- 44 57 Tmmmn—mTmmm 72 6.80 7.00 7.20 7.40 5000 m/z 43.05 53.15% 27
53 67 82 ।11111 02tt 4 - -TI T 11 mP 1‘‘2111111111711 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62815: Butanal, 3-methyl- 44 6.80 7.00 7.20 7.40 m/z 57.10 50.25% 5000- 58
71 38 49 86 l - ■ ■ ■ I ■ ■ ■. 11 ■.. I..111111' 111 f 11 '111''11 " 1' i " " r 1' ■ i ............... 1T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.80 7.00 7.20 7.40
9579.D GCMS0501.M Mon May 06 10:49:48 2002 Page 1
NYC-WTC_000046254
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024997
Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000046213
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 7-9 2002.
Filed in the same folder
NYC-WTC_000046214
Single page excerpt from a GCMS laboratory record file stored in DEP Box 25, dated between May 7 and May 9, 2002.
Filed in the same folder
NYC-WTC_000046217
Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
Filed in the same folder
NYC-WTC_000046226
Laboratory report of GCMS calibration analysis for sample AE09579 conducted on May 8, 2002, listing detection limits.
Filed in the same folder
NYC-WTC_000046230
Laboratory report of GCMS reference analysis for sample AE09579 conducted on May 8, 2002, showing response factors.
Filed in the same folder