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GC/MS analysis results for sample AD22778, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22778 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087682–000087693

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087690
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22778.D Vial; 15 Acq On : 3 Oct 2001 3:49 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 6.47 0.53 ug/1 62469 1,4-Dichlorobenzene-d4 11.79 Hit# Of Tentative ID MW MolForm CAS# Qual 1 2-Hex^one 100 C6H12O 000591-78-6 90 2 2-Hex/none, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 4 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 50 Sundance J, Scan 156 (6.471 min): 22778.D (-) m/z 43705 100.00% 43

58 5000

71 85 100 6.20 6.40 6.60 6.80 .................. . I''''I'''' I ' ' ' ' I ' ' ' ' I' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ' I ' ' m/z 58.05 58773% Ti/z-> 20 30 40 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 6.20L 640 a60 a8g m/z 41.00 17.26% 27 85 100 I 1 71 I n/z-> ^bundance 20 30 40

43 50 60 70 80 90 100 110 120 #11968: 2-Hexanone, 4-hydroxy-3-propyl-

58 J..................... 130 140

w _6;20__640__a60__63q^_ 29 m/z 56.95 12773%

....... ‘''l....... ' I''' ,1 ....... 140 TT/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ^bundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 6.20 6.^ 6.^ 6.80 58 m/z 100.00 10.47%

5000 71

30 85 100 aaA/a I ' ' I ' I ' nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22778.D NP091101.M Fri Oct 05 08:47:51 2001 Page 1 NYC-WTC_000087690

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NYC-WTC_000087690Source: NYC Law Department, mirrored locally

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