GCMS calibration table for method GCMS0412, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Nonanal Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.06 1.89 ug/1 296083 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonanal 142 C9H180 000124-19-6 (91) 2 Decanal 156 C10H20O 000112-31-2 45 3 Cycloheptane 98 C7H14 000291-64-5 27 4 3-Heptene, (E)- 98 C7H14 _____ 014686-14-7 22 Abundance Scan 982 (14.061 min): 8016.D (-) m/z 57.00 100.00% 41 57

5000 70 82 98 -.............. 13.80 14.00 14.20 14.40 ‘........ .. • r 'I' 151 I-r ri + H— । 114 124 ' r ■1 'i ■1 ’ ■ ।111 111 ■1111 ■1 ■ । m/z 41.05 83.64% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #66171: Nonanal 57

44 5000 98 TUTTI ■ ■ ■ i 70 82 13.80 14.00 14.20 14.40 27 m/ Z 43.05 66.84% 114 - 142 ■ ' i ' ' ■ i ■ 1 ‘ I’’ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11579: Decanal / 43 57 ‘111 13.80 14.00 14.20 14.40 m/z 56.00 56.53% 5000 70 82 1...... ?5......... 112.............................. 1 1 1 1 ■ 1 i 1 1 ‘ ' i 1 1 1 1 i 1 ■ 1 ■ i 1 1 ' ' i ■ 1 1 1 1 1 1 ' 1 I ' 1 1 1 I n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63231: Cycloheptane I I I 1 I I I I I P I I I I I I I I I 41 13.80 14.00 14.20 14.40 70 m/z 55.00 50.29% 27 98 5000 83

n/z-> 1 I ■ r ' 1 i ■ 1 ■ 'i1 20 30 40 —l — ' ' i 1 1 1 1 i ' ' 50 60 70 80 90 100 110 120 130 140 }t‘rTCTFTT"TUEIT/T/VTT /.................. 1 1 i 1 1 ' 1 r1 1 13.80 14.00 14.20 14.40 i 1 1 1 1 1 1 ' 1 |

8016.D GCMS0412.M Tue Apr 16 12:08:05 2002 Page 2 NYC-WTC_000047707