Laboratory report documenting GCMS analysis of sample AE11308 conducted on May 28, 2002, including surrogate recovery data.
NYC-WTC_000024987–000024996Folder label: “GCMS X 5/14/02 A 5/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\MAY2 102\11307.D Vial: 21 Acq On : 21 May 2002 8:29 pm Operator: Sample : EXTRACTS/14 Inst 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Oxetanol, 2,2,3-trimethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.92 0.57 ug/1 36721 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Oxetanol, 2,2,3-trimethyl- 116 C6H1202 025910-96-7 28 2 Acetone' 58 C3H60 000067-64-1 25 3 Acetig' acid, 1-methylethyl ester 102 C5H10O2 000108-21-4 17 4 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 Abundance 7 Scan 532 (9.920 min): 11307. D (-) m/z 43.00 100.00%| 43
5000
58 87 1 1 i ■ ■ 98 9.60 9.80 10.00 10.20
m/z—> i " " r ' " i1' " i a +1+ 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 r '1111'111'1 '11' ।111''1' r 11 ■ i' • ‘' r 1 m/ z 58.10 23.05% Abundance #3281:3-Oxetanol, 2,2,3-trimethyl- 43
5000 58 9.60 9.80 10.00 10.20 71 m/z 87.05 15.27%| 27 86 i " 111 ‘ ' J " ' r " 11" " i " r 11'1 T-rp-r m " I'1 T-HHH m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62322: Acetone 43 '■ 1 I ' ' . A... T I I I I I I I I I I I I I— I I I T 9.60 9.80 10,00 10.20 5000 m/z 59.10 11.42%| A 58 27 " | " । । | I H 1 | ■ । । । [T-r-T-i | I I 11" ■' r " 11 1’12’1111-1110111111""1 ’’—0—1100E——0B331"T iz—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1719: Acetic acid, 1-methylethyl ester T 1, I ll I I I II I I I I
43 9.60 9.80 10.00 10.20 m/z 98.10 8.44% 5000
61 27 87 -H + H i" " i - T ■1111'111 1 1 i ■ 1 1 1 i 1 ' ' r1 1 1 1 । 1 1 1 1 i m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 9.60 9.80 10.00 10.20
11307.D GCMS0520.M Wed May 22 09:20:51 2002 Page 2
NYC-WTC_000024995
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NYC-WTC_000025031
Laboratory report documenting GCMS analysis of sample AE11378 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025041
Laboratory report documenting GCMS analysis of sample AE11379 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025012
Laboratory report documenting GCMS analysis of sample AE11310 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024977
Laboratory report documenting GCMS analysis of sample AE11307 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023728
Instrument log and analysis summary for GCMS testing of sample AE10065 conducted on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025022
Laboratory report documenting GCMS analysis of sample AE11377 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022688
Laboratory report presenting analytical data for environmental sample AE11797 and surrogate recovery metrics.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023708
Instrument log and analysis summary for GCMS testing of sample AE10064 conducted on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023691
Instrument log and analysis summary for GCMS testing of sample AE10063 conducted on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023674
Laboratory report page showing GC/MS analysis for sample AE10062 including surrogate recovery data on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022670
Laboratory record of analytical results for environmental sample AE11795 with surrogate recovery information.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012673
Laboratory record from May 30, 2002 documenting the recovery of surrogate standards for sample AE11573.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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Laboratory report of a method blank analysis for GCMS testing conducted on May 21, 2002, showing non-detects for various compounds.
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Calibration report for GCMS analysis of sample AE11306 performed on May 21, 2002, listing response factors for target analytes.
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Reference standard analysis report for GCMS testing of sample AE11306 conducted on May 21, 2002, verifying instrument performance.
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