GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Eicosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.59 0.31 ug/1 40837 Acenaphthene-dl0 21.29

Hit# of 5 Tentative ID MW MolForm CAS# Qu al

1 Eicosane 282 C20H42 000112-95-8/91 . 2 Heptadecane 240 C17H36 000629-78-790/ 3 Tetradecane 198 C14H30 000629-59-4 87 4 Hexadecane 226 C16H34 000544-76-3 80 Abundance Scan 1911 (22.590 min): 1462.D (-) m/ z 57.00 100.00% 7 43 71 5000 85 TET fl 1 1 1

—l _113................ 22.20 22.40 22.60 22.80 23.00 i1 11' 11 1 I1 ' ' 'I'' 1 1 1 1 1 '11 1 1 1 1 I 1 11 1 I 1 1 1 1 1 1 m/ Z 43.05 68.00% miz-> 20 40 60 80 100 120140160180200 220 240 260 280 Abundance #72323: Eicosane 43 57

71 1 A 1 1 1 1 A —AAA 4 — aa । 5000 ; 85 22.20 22.40 22.60 22.80 23.00 m/z 71.10 57.38% - 89 113 127 141 282 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 43 57 ................ . 1 ■ 1 1 1 71 22.20 22.40 22.60 22.80 23.00 5000 m/z 41.05 40.46% 85

, 99 113 127 141 240 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69661: Tetradecane —........... -AAA 43 57 22.20 22.40 22.60 22.80 23.00

71 m/ z 85.05 36.27% 5000- 85

27 , I ! —- 99 113 155 198 i ' ’ 1 ' i ' ' 1 1 1 1 H ' 1 ' ' I 1 1 ' ' I ‘ ' 1 ‘ I 1 1 ' ' I ’ ' I 1 ' ' ' 1 1'1 ' 1 I 1 1 .................. — TII । • i । । । । m/z->20 40 60 80 100 120 140 160 180 200 220 240 260 280 22.20 22.40 22.60 22.80 23.00

1462.D GCMS0308.M Mon Mar 25 08:27:29 2002 Page 4

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