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GC/MS analysis results, sample AE09770, May 15 2002

Machine-extracted title · confidence 100%

Laboratory report page showing GC/MS analysis for sample AE09770 including surrogate recovery data on May 15, 2002.

NYC-WTC_000023621–000023634

Folder label: “GCMS X 5/9/02 A 5/10/02

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Scanned page image, NYC-WTC_000023632
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1002\9770.D Vial: 12 Acq On : 10 May 2002 11:47 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 4 Eicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

27.75 0.77 ug/1 81036 Phenanthrene-dl0 25.55 Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Eicosane 282 C20H42 000112-95-8 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Nonadecane 268 C19H40 000629-92-5 90 4 Hexatriacontane__________________ 507 C36H74 000630-06-8 87 Abundance Scan 2478 (27.750 min): 9770.D (-) m/z 57.10 100.00% 57 43 71 5000 85

27.40 27.60 27.80 28.00

m/z-> J60 h ' ' i ' 40 99 113 127 141 155168 91—10] 100 120 140 160 180 200 220 240 260 280 m/z 43.10 78.08%| Abundance #72323: Eicosane 43 57

71 5000 85 27.40 27.60 27.80 28.00 m/z 71.15 63.52%| — 11 99 113 127 141 4 1 1, ' d ■ 282 ' I ' ' ‘ ' I ' ' ‘ ' I ' ' ' ' I ' ' ‘ ’ I ' ' ' ' I ■ ■ ' ' I ' ‘ ' I ' ' ‘ ' I ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 57 43 WA n 71 27.40 27.60 27.80 28.00 5000 m/z 85.15 38.54%| 85

mz-> 1111 40 J 99 113 127 141 TuBII r iido 240 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #37469: Nonadecane DAT MA r *T ' ‘ ' I ' 57 27.40 27.60 27.80 28.00 43 71 m/z 41.05 35.77%| 85 5000

99 — — 113 127 183 197 268 ■ - I ' ■ Iiji’ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 27.40 27.60 27.80 28.00

9770.D GCMS0510.M Mon May 13 12:10:26 2002 Page 4

NYC-WTC_000023632

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NYC-WTC_000023632Source: NYC Law Department, mirrored locally

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