GC/MS analysis results, sample AE09770, May 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\MAY1 002\9770.D Vial: 12 Acq On : 10 May 2002 11:47 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 Triacontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 28.93 0.58 ug/1 60270 Phenanthrene-dl0 25.55 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Nonadecane 268 C19H40 000629-92-5 90 4 Heptadecane 240 C17H36 000629-78-7 90 Abundance Scan 2607 (28.932 min): 9770.D (-) m/ z 57.05 100.00% 57

5000 85

■ i ' ' ■ ' i ' ■ ' ■ i 28.60 28.80 29.00 29.20

miz-> IWA 113 141 206 TTHTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTITTTITTTTTTTT 40 60 80 100120140160180200220240260 280300320340360380400420 m/z 43.05 69.99% Abundance #55461: Triacontane 43 71 5000 28.60 28.80 29.00 29.20 m/z 71.20 59.83% , । 99 197 II... ndalr 239 267 TTTPmuE-0T’m31-B1-1"113 1‘:17111111‘11113111117"11111111711111111110391103001001311-—2033337TT 379 422 miz-> 40 60 80 100120140160180200220 240260280300320340360380 400420 Abundance #72323: Eicosane 57 — __ _J I_ — —_ TYTTYTRTTPAAY 28.60 28.80 29.00 29.20 5000 m/z 85.15 41.25% 85

mz-> — a- i i113 141 282 ■ ■ i" " i' ‘" i" ■' i" " i" " i" " i" “ i" " i" " i" " i'1" r11' i" " i ■" ■ i ■" 40 60 80 100120140160180200220240260 280300320340360380400420 Abundance #37469: Nonadecane A A , AA 4/AA MA 57 28.60 28.80 29.00 29.20 m/z 41.10 32.85% 85 5000

m/z—> 11 ■ i''' L 113...... 183....... 268 TTTTT Tt’B’1’11—2211—2411444414444181148 "i""i r ■" i 40 60 80 100120140160180200220240260280300320340 360 380 400 420 28.60 28.80 29.00 29.20

9770.D GCMS0510.M Mon May 13 12:10:27 2002 Page 5

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