GCMS analysis results for sample AE07312, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0302\7312.D Vial: 8 Acq On 3 Apr 2002 7:35 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Tritetracontane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.93 0.22 ug/1 36342 Phenanthrene-dl0 25.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tritetracontane 605 C43H88 007098-21-7 6 2 Nonadecane 268 C19H40 000629-92-5/87 3 Tetracosane 338 C24H50 000646-31-1 86 4 Tricosane________ 324 C23H48 000638-67-5 86 Abundance Scan 2058 (23.935 min): 7312.D (-) m/z 57.00 100.00% 57

5000 85 C- I |I Ai AI 1 I | 1 I / I I\/ | I 1 TA I 1 | I I I I |

23.60 23.80 24.00 24.20 ■ i 1 1 । 1113141 m/ Z 43.05 67.91% m/z—> 501 100 150 200 250 300 350 400 450 500 550 600 Abundance #60913: Tritetracontane 57

5000 85 wa AA m 4A / Vwn 44 , 23.60 23.80 24.00 24.20 m/z 71.00 61.29%

m/z-> ■ 1 i

50 1 114 100 150 196 463491 519547 576604 ' i 1 1 ' 1 i 1 ' ■ ' i ■ ' ' 1 i ' ' ' ■ i 1 ' 1 1 i 1 1 ‘ 1 I 1 1 ' ■ i 1 ' ■ 1 i 1 ■ 200 250 300 350 400 450 500 550 600 Abundance #37469: Nonadecane 57 n..../ V .... 23.60 23.80 24.00 24.20 85 5000 m/z 85.05 45.94%

1113 183 268 1 ' i 1 m/z-> Abundance 50

57 100 150 200 250 300 350 400 #73543: Tetracosane 450 500 550 600 — 23.60 23.80 24.00 24.20 L 1nd 1" I I I I I I J

m/z 41.05 35.56%

5000 85

| | 113 155183 294 338 *‘1117/171/171/4/1/11/*1/1‘/‘‘1/I/TI1/1/*-/I/-/1‘‘‘‘I‘‘‘‘I‘‘IIIIIIII AMAAAA I i | i i । I | i I । i । ill i । I i i r I

m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 23.60 23.80 24.00 24.20

7312.D GCMS0403.M Tue Apr 09 13:07:52 2002 Page 2

NYC-WTC_000046621