GCMS analysis results, sample AE02785, March 2002

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Data File C:\HPCHEM\1\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 3

R.T. EstConc Area * Relative to ISTD R.T.

39.22 1.59 ug/1 164668 Perylene-dl2 38.06

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacont;ane 507 C36H74 000630-06-8 91 2 Tritetracontane 605 C43H88 007098-21-7 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 3723(39.223 min): 2785.D (-) .......................... 1 m/z.... 57.00...... 100.00% 57

85 5000

m/z~> 1 r i' 50 11120 100 150 200 250 300 350 400 450 500 550 600 38.80 39.00 39.20 39.40 39.60 m/z 43.05 73.29% Abundance #74635: Hexatriacontane 57 5000 85 i 38.80 39.00 39.20 39.40 39.60 : m/z 71.00 71.70%

m/z-> 1 ■ I' 50 1 113141,196 225253281 100 150 200 250 300 350 400 450 500 550 600 Abundance 57

38.80 39.00 39.20 39.40 39.60 5000 85 m/z 85.0 52.11%

111 141 196 46349-1519547 576604 m/z-> .. 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74745: Tetratetracontane _ TM,/A Al.... AT 57 38.80 39.00 39.20 39.40 39.60 m/z 55.00 30.09% 5000 85

1113141........................................... 463491519547 591618 1 ' 1 1 m/z-> 50 100 150 200 250 300 _ 350 400 450 500 550 600 38.80 39.00 39.20 39.40 39.60

2785.D GCMS0208.M Tue Mar 05 10:51:04 2002 Page 9

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