GCMS analysis results, sample AE02785, March 2002

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Data File C:\HPCHEM\1\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexadecane, 1-chloro- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

40.61 0.55 ug/1 56755 Perylene-dl2 38.06

Hit# of 5 MW MolForm CAS# Qual

1 Hexadecane,/1-chloror 260 C16H33C1 004860-03-1 72 2 Octadecane, 1-chlor 288 C18H37C1 003386-33-2 56 3 Pentadecane 212 C15H32 000629-62-9 47 4 Pentacosane 352 C25H52 000629-99-2 45 Abundance Scan 3874 (40.609 min): 2785.D (-) m/z 57.0, 100.00% 57

43 71

5000 85

97 — '■<ji.1•।■■■■।1113............. ■ i • 1 ' ' i ’ > ’ ■ i ■ ■ ■ • i ■ ■ 1 1 I 1 > 1 1 I 1 1 ‘ ' I 1 1 1 ' I 1 1 40.20 40.40 40.60 40.80 41.00 m/z 71.10 ~ 69.13% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71719: Hexadecane, 1-chloro- 57

5000 71 91 vMww Al,, mTwry

“M 40.20 40.40 40.60 40.80 41.00 105 I II x,I 1119 133 ' ' 1 ' I ' ’ ' ‘ I * ' ' 1 I ' ' ' 233 260 1 | 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 1 1 1 m/z-40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 57

c 40.20 40.40 40.60 40.80 41.00 5000 71 m/z 85.05 48.60% 91

105 . 119 133 261 288 m/z-> Abundance 40

43 57 60 80 100 120 140 160 180 #70278: Pentadecane 200 220 240 260 ............................ 280 AAAAAA 40.20 40.40 40.60 40.80 41.00 m/z 40.95 33.30% 71 5000- 85

m/z-> — 40 60 ' 1 1 1 80 . 99 113 127 141 155 169 100 120 140 160 180 200 212 220 240 260 280 JAOMAMIL" 40.20 40.40 40.60 40.80 41 ^00

2785.D GCMS0208.M Tue Mar 05 10:51:09 2002 Page 10

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