GCMS analysis results for sample AE08951, May 2002

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Laboratory report documenting GCMS analysis of sample AE08951 conducted on April 29, 2002, including detection of unknown compounds.

NYC-WTC_000043619–000043631

Folder label: “GCMS X 3/26/02 No Analyses”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0602\8951.D Vial: 8 Acq On 6 May 2002 11:10 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Nonadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.24 0.63 ug/1 60169 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane 268 C19H40 000629-92-5 53 2 Eicosane 282 C20H42 000112-95-8 49 3 Tricosane 324 C23H48 000638-67-5 49 4 Docosane 310 C22H46 000629-97-0 49 (Abundance / Scan 2204 (25.240 min): 8951. D (-) m/ z 57.10 100.00% 57 43 71 5000 85 192

25.00 25.20 25.40 25.60 11 | 199113............. i । । । । । i । । । I I | i i i i | i i । । । I I i । | i r 1 । i । । i । । । i i । । । i । । । । n । । i । । । । i i । । i । m/z 43.15 80.84% m/z->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #37469: Nonadecane 57 43 71 85 5000 ■ ' i ' 25.00 25.20 25.40 25.60 m/ Z 71.20 64.60%

m/z-> LL40 60 80 99 J 113127 183197 268 1 । । I1 i । i \ । i [ । i । । । r i~r i । । । । i । , i i t । i i r i । । । i i । i I i । । 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #72324: Eicosane 43 5(7

71 A A m/ Z A W A. 25.00 25.20 25.40 25.60 85.15 41.23% 5000 85

99 .. ,, I,, I , III.,, II,, 1J11 113 141155169 183197 254 282 '1 I1'' 1 11 ' ' 1 1 1 1 1 ■1111111111' ■ i ■'1 11'1'111 1 ‘' i 1'111 ■'11 i1111 rr ■' ■ i'' ■111 ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane M A.......... l...... -444 I I I I I I I I I I I I I I I I 43 57 25.00 25.20 25.40 25.60 m/z 192.05 40.82% 71 5000 85

' ' I ' ‘ 11 11 ' I 28 113127141 i' 1111 183197211225 110011—00111107110111un—ni 296 324 1 1 1 1 1 " I 1 1 ' 1 i 1 ' i ■ ■ ■ ■ i ■ ■ ■ < i ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 25.00 25.20 25.40 25.60

8951.D GCMS0501.M Wed May 08 11:51:41 2002 Page 3

NYC-WTC_000043628

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NYC-WTC_000043628Source: NYC Law Department, mirrored locally

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