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GCMS analysis results for sample AE01503, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01503 conducted on March 6, 2002.

NYC-WTC_000003591–000003606

Folder label: “GCMS X 1/23/02 A 2/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Nonadecane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

24.03 0.42 ug/1 36974 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Nonadecane 268 C19H40 000629-92-5 0 2 Pentadecane 212 C15H32 000629-62-9 87 3 Eicosane 282 C20H42 000112-95-8 86 4 Heptadecane 240 C17H36 000629-78-7 78 Abundance Scan 2068 (24.030 min): 15biD (-)....................... m/z 57.00. 100.00% 57 43 71 85 5000

99 ATT —44 P14 23.60 23.80 24.00 24.20 24.40

m/Z-2 —Tr I ■ ■ 40 60 1—80 100 120 140 160 180 200 220 | 113 127 140 155 ' ■ i ' ' ' ' i ' '■ ■ ' I ' ' ' '■ i ' ■ ■ ' i ' ' ' ■ i ' ' ' ' i 1 ' ' ‘ i ' ' ' ' i ■ ■ 240 260 280 m/z 43.00 77.65% Abundance #37469: Nonadecane 43 57 71 85 LA---A--AAAA 5000 •AAAAA 23.60 23.80 24.00 24.20 24.40 m/z 71.10 68.54% 99 113 127 183 197 268 ■111111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance *26001 erad —

43 57 \ 71 ...... V,.... 23.60 23.80 24.00 24.20 24.40 5000 85 m/ z 85.05 54.25%

99 . 113127 168 212 m/z->. Abundance 40 43 57 60. . 80. 100 120 140 160 #72324: Eicosane 180 200 220 240 260 280 A.... .. 23.60 23.80 24.00 24.20 24.40 m/z 41.05 38.63% 71 5000 85

TTTTTt 99 113 III I 141 155 169 183 197 254 282 AAA-A 44444 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 23.60 23.80 24.00 24.20 24.40

1503.D GCMS0208.M Tue Feb 26 15:12:46 2002 Page 3

NYC-WTC_000003600

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NYC-WTC_000003600Source: NYC Law Department, mirrored locally

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