Laboratory report documenting GCMS analysis of sample AE01503 conducted on March 6, 2002.
NYC-WTC_000003591–000003606Folder label: “GCMS X 1/23/02 A 2/22/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 4 Bitoscanate Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
25.38 0.35 ug/1 31451 Phenanthrene-dl0 25.74
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Bitoscanate 192 C8H4N2S2 004044-65-9 35 2 Nonadecane 268 C19H40 000629-92-5 25 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 22 4 _Pentadecane 212 C15H32 000629-62-9 22 Abundance < Scan 2215 (25.380 min): 1503.D (-) m/z 192.00 100.00% 57 192
43 71 5000- 85
146 160 25.00 25.20 25.40 25.60 25.80 —T— 1.. m/z 57.00 98.75% m/z-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #20576: Bitoscanate 192
5000 , [4M4 m M4n n 25.00 25.20 25.40 25.60 25.80 134 90 160 m/z 43.05 60.93% 63 76 THr 1 ■ • j • ■ ■ ■ 11 • ■ ■ । ■ 1 . 107 148 m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 43 57 71 vM M M WMN A A rw 25.00 25.20 25.40 25.60 25.80 85 5000 m/z 71.00 56.07%
99 113 127 183 197 268 m/z-> Abundance 40. 60. 80__ 100 120 140 160 180 200 220 240 260 280 300 #42196: Heptadecane, 2,6,10,15-tetramethyl- AAAALAA -A— 57 71 25.00 25.20 25.40 25.60 25.80 m/ Z 85.05 45.66% 5000 85
1 1 i ■ ■ 99 113 Il ■. 'I1, 127 141,155 ., 183 ,. 211 .... . . 296 A A.. I AM , , / 1 1 1 1 f ' l ' 1 1 ' I < " ' I • ’ ' IT m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 25.00 25.20 25.40 25.60 25.80
1503.D GCMS0208.M Tue Feb 26 15:12:50 2002 Page 4
NYC-WTC_000003601
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