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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088414
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D Vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 2 09 G7VLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Eicosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.62 1.32 ug/1 139325 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 91 2 Docosane 310 C22H46 000629-97-0 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Pentadecane 212 C15H32 000629-62-9 91 Abundance Scan 2678 (29.623 min): 23318.D (-) in/z 57700 100.00% 5(7 43 71

5000 85

A 99 29,20 29.40 29,60 29.80 30.00 J' I'' ■' I' ' .. f...I' f ■ ■ I 207 310 . I... pTT-T-T-p-TT-TyT-T-TT-Y-r^^ m/z71.10 67.09% TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #39862: Eicosane 43 57

71

5000- 85 mA. A 29.20 29.40 29.60 29.80 30.00 m/z 43.05 66772%

Ti/z-> 40 60 u T.80 196 ‘I ' ' " I I'■I>I 1 I I I I 240 • I'''' J *' '' I ■'■n" 100 120 140 160 180 200 220 240 260 280 300 282

Abundance #72997: Docosane 43 57 JU7 29.20 29.40 29.60 29.80 30.00 71 5000- m/z 85.05 47.26% 85

■n/z-> 40 UUL 113127 155169183197211 60 80 100 120 140 160 180 200 220 240 260 280 300 292 310

Abundance #71560: Octadecane / 43 57 29.20 29.40 29.60 29.80 30.00 "m/z 41.05 30.78% 71 55H 85

99

Tl/Z-> 40 60 I, I J 169183197210 /4-rY4^-r-j*YrT-lHq-TA-T-qh-rT-T-yrTH-Tqp-T--rT^^

80 100 120 140 160 180 200 220 240 260 280 300 254 I ' ' ' ' I ' ' ' ' I '.. J.Va.a.. 29.20 29.40 29.60 29.80 30.00

23318.D NP091101.M Mon Oct 15 09:45:52 2001 Page 6

NYC-WTC_000088414

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NYC-WTC_000088414Source: NYC Law Department, mirrored locally

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