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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088146
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23263.D Vial: 9 Acq On : 9 Oct 2001 9:11 pm Operator: 2 09 GTkLOS Sample : g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Eicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 30.70 0.67 ug/1 143856 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 93. 2 Heneicosane 296 C21H44 000629-94-7 91 y 3 Tetracosane 338 C24H50 000646-31-1 90/ 4 Nonadecane 268.. C19H40 000629-92-5 90/ Abundance Scan 2795 (30,701 min): 23263,D (-) m/z 57700 100.00% 57

43 71

85

■n/z-> J “TTp- 40 J J J■?

60 J,^^169183.

80 100 120 140 160 180 200 220 240 260 280 300 320 340 30,40 30,60 30,80 31,00 m/z TIToO ft 67.50% ^bundance #72323: Eicosane 43

71 Mia 1”' '

85 30,40 30,60 30,80 31,00 m/z43.05 64.36% I T ^13127141 282 pn‘’’hyMVTTyT-r1hnp-WT-^ Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 30,40 30,60 30,80 31,00 5000 m/z 85.05 47.52%

99 il J I • I I I J T I I r I I I T 1 I I I I I I . I I I I i I I . I I . I I I I I I Tp I ’l I I 268 296 I ‘" I' " 11' T ii/z-> Abundance 40 60

43 57 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane L rVj 30.40 30.60 30,80 31.00 71 m/z 41705 26.18%

5000 85

uu 99 l| 155169183197 ■ 294 338 ' I'''' I " ‘' I'' ' I' ‘ T'' I''' I' ' ' 'I ' 71/Z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30,40 30,60 30,80 31,00

23263.D NP091101.M Thu Oct 11 10:50:37 2001 Page 5,

NYC-WTC_000088146

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NYC-WTC_000088146Source: NYC Law Department, mirrored locally

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