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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088147
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23263.D Vial: 9 Acq On 9 Oct 2001 9:11 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 3 I R.T. EstConc Area • Relative to ISTD R.T. 31.65 1.47 ug/1 312753 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual CZ^Butyl tetradecanoate (myristate) 284 C18H36O2 : 000000-00-0 80 2 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 ■3 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 4 2-Methyl-N-1-tridecene 196 C14H28 018094-01-4 27 Abundance Scan 2898 (31.646 min): 23263.D (-) m/z 56700 100.00% 50 ft 5000 4 73 129 T vA 101 1 2£21324i267^ 31.40 31.60 31.80 32.00 ,153 340 I'''' I I " '' I " " I " '' I' " ' I'''' I' I '' I'' m/z 56795 7744% nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #40186; Butyl tetradecanoate (myristate) 53

5000 229 n ' 'T 31.40 31.60 31.80 32.00

Ti/z-> ^bundance 20 40 u 60 73 129 211

I '' ' ' I' ‘ ' I ''' ‘ I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #5067; Oxirane, 2,3-bis(1-methylethyl)-, trans- 284 m/z 43.05 42.22%

5 5- 41 31.40 31.60 31.80 32.00 5000 m/ Z 41.05 34.27% il 73

n/z-> 20 40 60 A 113128 1 ''' ' I ' ‘ ' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Aibundance #1354:1-Hexene, 2-methyl- ^^1 53 31.40 31.60 31.80 32.00 m/z 73700 29.72% 41 5000

Ti/z-> 20 I 83 5^ ' ' '"I ‘ ‘ ' I ' T I'''' I'''' I'''' I'''' r '' ‘ I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 T V 31.40 31.60 31.80 32.00

23263.D NP091101.M Thu Oct 11 10:50:39 2001 Page 6

NYC-WTC_000088147

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NYC-WTC_000088147Source: NYC Law Department, mirrored locally

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