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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088145
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23263.D Vial: 9 Acq On 9 Oct 2001 9:11 pm Operator: 209 GALOS Sample g c/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************************** Peak Number 4 Hexatriacontane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 29.63 0.44 ug/1 93474 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91x^ 2 Tricosane 324 C23H48 000638-67-5 91 / 3 Heptadecane 240 C17H36 000629-78-7 91 / 4 Octadecane 254 C18H38 000593-45-3 91' Abundance Scan 2678 (29.627 min): 23263.D (-) m/z 57.00 100.00% c

43 71 85 5000

I I 99 29.20 29.40 29.60 29.80 30.00 ■ Il I .1 I, J ^J3^?7141155169183 p V IVj 1 ‘i l , jT. « I I r«-T I I .1 , , p , . s J < t I » I , 1 V 1 I I ' ' ' ' I ‘ ' I ' ’ ' ' I ' '' ' I ’ ' ’ ' I “mTz 71.10 70711% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #74636: Hexatriacontane 43 5 7

5000 71 85 A A A. 29.20 29.40 29.60 29.80 30.00 m/ Z 43.05 65.84% 1 !|^21^''?^141 155169183197211 I' ' ' ' I ' ' r' I ' ' ' ' i' I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' i I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57

71 29.20 29.40 29.60 29.80 30.00 85 "mTz 85.05 49.83% t

ijtew p ' ' 'I ' '‘'I‘ ' I ' 183197211225 I ‘ ' I ' ' ‘ ' I ' ' ' ' I 296 ''' r ''' P ' 324 •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193: Heptadecane Lx-Zk T“' '"f 'I 7 29.20 29.40 29.60 29.80 30.00 “m/z 41705 26796% 71 553 85

99 J ’'^■'27141155169 210 240 TTTT ' I ' ''' I' ' I I ' r' I ' I I ' I'' ' ' ' I ' ' I I I I' ' ‘ ‘ I''' ' I.' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 29.20 29.40 29.60 29.80 30.00

23263.D NP091101.M Thu Oct 11 10:50:35 2001 Page 4

NYC-WTC_000088145

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NYC-WTC_000088145Source: NYC Law Department, mirrored locally

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