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GC/MS analysis results for sample AD23345, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.

NYC-WTC_000088556–000088584

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088575
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23345.D vial: 17 Acq On : 10 Oct 2001 4:57 am Operator: 209 GTVLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Eicosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 32.73 6.72 ug/1 588340 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91, 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 90 4 Tetracosane __ ________________________ 338 C24H50 000646-31-1 90 Abundance Scan 3016 (32.731 min): 23345.D (-) m/z 56795 100.00% 57

5000 85

4 32.40 32.60 32.80 33.00 ■A ..y, .. .225 253 281 352 n I I p I . . T I i r I I p . I i‘ I . ri . I I . . , p . . . I , , , , J , , m/z71.00 69.30% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862; Eicosane 57

5000 85 32.40 32.60 32.80 33.00 m/z 43.05 66781% I 141 1 1 196 240 282 I ' '' ' I '' ' ' I' ' '' I T-rp-m-j- I' '' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57

85 II ' T 32.40 32.60 32.80 33.00 m/z 85.05 49.48%

..(J jjr.T................ 224. 254....................... Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 32.40 32.60 32.80 33.00 Wz 41.00 22.86% 85 5000

268 296 iYrTTTp"rT7-pTTT-*rp I'''' I'''' I T" ' ' I " '■'T' I' ' '^T" ' ' I rT=|-r‘i=n-pj"F“erTf=p=^^ 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23345.D NP091101.M Thu Oct 11 13:10:35 2001 Page 13

NYC-WTC_000088575

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NYC-WTC_000088575Source: NYC Law Department, mirrored locally

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