GCMS analysis results, sample AE05152, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\5152.D Vial: 38 Acq On : 31 Mar .2002 5:40 am Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table ) Library : C:\DATABASE\NBS7 5K.L ********************************************************************* Peak Number 4 Piperidine, 1-acetyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

13.52 0.35 ug/1 46986 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Piperidir/e, 1-acetyl- 127 C7H13NO 000618-42-8 33 2 2-Methylpiperidine 99 C6H13N 000109-05-7 33 3 1-Pyrrol idineethanamine 114 C6H14N2 007154-73-6 28 ~ Propanamine, 2-methyl-N-(2-methyl 127 C8H17N ________ _0^6898j82_-4 25 Abundance Scan '923 (13'522 minTsiSZ.D (-) ‘ .................... .. m/ z 84.0.0 ‘"’1 do”.’ 6 d%. i

42 5000 126 141 -6 71 I, 98 .......... Illll .... .... Il.. I m/z 13.20 13.40 13.60 13.80 42.05 50.20% ■ m/z->___ 20___ 30_... 40_ 50 60 70 80 90 100 110 120 130 140 Abundance #4779: Piperidine, 1-acetyl- 8U

127 56 5000 70 42 13.20 13.40 13.60 13.80 27 m/z 12’6. TO 38.77% ' Ui m/z->____ 20___ 32 40 50 60 70 80 I 99 112 I, , I, , , i'l___ I I , , ,-p-4, I . . . . I , , 90 100 110 120130 140 Abundance #63287: 2-Mettiyipiperi<jir>e i 84 . ............ .......................................... I 13.20 13.40 13.60 13.80 ' 5000 42 56 m/z 44.05 29.81% 30 70 99

m/z-> 20 30 40 50 60.. 70. 80__ 90 100 110 120 130 140 Abundance #2949: i-Pyrrolidineelha’namine ......................... a# 13.20 13'4'0' '13'60 13'30 ' ' ' m/z 41.05 22.17% 42 5000

30 56 70 114 20 30 40 50 60 70 80 90 100 110 120 130 140 13.20 13.40 13.60 13.80

5152.D GCMS0308.M Tue Apr 02 15:39:58 2002 Page 4

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