GC/MS analysis results, sample AE10605, May 10 2002

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Laboratory report page showing GC/MS analysis for sample AE10605 with non-detect results on May 10, 2002.

NYC-WTC_000023580–000023593

Folder label: “GCMS X 5/9/02 A 5/10/02”

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Data File : C:\HPCHEM\1\DATA\MAY1002\10605.D Vial: 7 Acq On : 10 May 2002 6:55 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise . Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************* * * ****************************** Peak Number 5 IH-l,2,4-Triazol-5-amine, 1-pr Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

13.76 0.90 ug/1 71503 1,4-Dichlorobenzene-d4 12.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual I 1H-1,2,4-Triazol-5-amine, 1-propyl- 126 C5H10N4 058661-96-4 35 2 1-Pyrrolidineethanamine 114 C6H14N2 007154-73-6 28 3 1-Butanamine, N-butyl-N-nitro- 174 C8H18N202 004164-31-2 25 41-Azetidinecarboxaldehyde,2,2,4,4-141C8H15NO 050455-46-4 25 Abundance Scan 952 (13.761 min): 10605.D (-) m/z 84.10 100.00% 42 84

5000 126 141 56 69 98 13.40 13.60 13.80 14.00

mz-> sillgaso ■ ■ ■ ■ i ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 42.05 11 ■1 ■ ‘ i i ■''111 ■' ■ i 11 81.04% Abundance #4408:1H-1,2,4-Triazol-5-amine, 1-propyl- 84

5000 97 126 13.40 13.60 13.80 14.00 43 55 70 rn/z 44.05 44.92% 111111111'11■11 ■11' i ■' i-q-i- '11 i ■' ■ ■ i " ‘11'1 ' I ' ' ' ' I 1 1 1 ' I ' 1 “ I 1 ' 1 1 [ II m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance ;#2949:1-Pyrrolidineethanamine 84

13.40 13.60 13.80 14.00 42 5000 m/z 126.15 38.36%

30 56 70 1.................. 114.................................................. m/z—> 1... 1..... 1 11,..... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #16148: 1-Butanamine, N-butyl-N-nitro- 1 84 13.40 13.60 13.80 14.00 m/z 41.15 34.47% 42 5000 131

56 72 174 ’ ’’I’ TTTT I 1 199 112......1,,.. ■ i ■r ■111 “ ■ i1 ■ ■ ■ । ■ ■ ‘111 ■' mz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 13.40 13.60 13.80 14.00

10605.D GCMS0510.M Mon May 13 09:31:55 2002 Page 5

NYC-WTC_000023591

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