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GCMS surrogate recovery data for sample AE07765, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07638 analyzed on April 18, 2002.

NYC-WTC_000040269–000040278

Folder label: “GCMS X 4/3/02 A 4/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APRI102\7765.D Vial: 14 Acq On : 12 Apr 2002 3:10 am Operator: Sample : gc/ms scan 4/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.83 1.11 ug/1 148610 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual i_ _ _ ..... ________ 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 2 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 3 Benzeneethamamine, N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 N-(Trifluorpacetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 1065 (14.826 min): 7765.D (-) m/z 73.00 100.00% 73 I

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 , L 323 . ' ■' I1 Tr ' T rt “ ' l"1 r 1 " T r m/ z 2 67.00 39.60% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 ........ \......... 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 35.66% .......................... 207 | 323 1 1 1 mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 4 14.40 14.60 14.80 15.00 15.20 5000 m/ z 356.05 13.34% (I 45 , 1 , ...... 1 1 I ' ' ' 1 i ' ' 208 251 281 ' i ' ' 1 ' i ‘ ' 1 i 386 458 548 ' l 1 1 ' 1 l ‘ ' ' T i Tna ' 1 1 r1 1 1 ■ 'i 1 r m/z—> 50 .100 150 200 250 300 350 400 450 500 550 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.40 14.60 14.80 15.00 15.20 m/ z 2 68.00 9.54% 5000 267 44 _ h.... 1 1 1 1 11 ' I ' ' 151 179 209 237 । 1 1 1 1 । 1 1 TII -i । । । । । । m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

7765.D GCMS0412.M Fri Apr 12 09:28:01 2002 Page 1

NYC-WTC_000040276

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NYC-WTC_000040276Source: NYC Law Department, mirrored locally

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