GCMS surrogate recovery results, sample AE01143, March 4, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\1143 .D Vial: 65 Acq On : 24 Feb 2002 8:04 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.92 1.26 ug/1 103830 Naphthalene-d8 15.97

Hit# Of 5 Tentative ID MW MolForm CAS# Qual --------------------- f---------------- 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 56 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 43 3 Benzeneethanamine , N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 4 3,4 -Dihydrox enzyl alcohol,tris (tr 356 C16H32O3Si3 068595-79-9 43 Abundance Scan 1076 (14.921 min): 1143.D (-) i m/z 73“ 00 100.00% 73

5000 267 355 45 ! 14.60 14.80 15.00 15.20 125 154 193 223 TInmndmnTTTT1 j 323 t....... | m/z 267.00 33.63% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 28.31% 1,.27m 323 m/z->____ 50 100__ 150 200 250 300 350 400 450 500 550 Abundance' ’ ' • b rn. 73 355 14.60 14.80 15.00 15.20 5000 m/z 356.0 9.58% 45 147 179 223 267 297 **1/n/——/n/n//n/n//0///1///0//*//1///n//—*////—/0//—//*/1/1/0//n)/B.n m/z-> 50 100 150 200 250 300 350 400___ 450 __ 500 550 Abundance #74706: Benzeneethanamine, N-i(pentafiuorophenyi)methylene] 73 355 14.60 14.80 15.00 15.20 m/z 267.90 9.16% 5000

45 208 251 281 386 458 548 ' ‘I * • —IWITTTTTTTT । * n • ■ ■ । ■ ■ • ■ । ‘ । 1 ■ ■ ■ 'i ■' r/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

1143 .D GCMS0208.M Fri Mar 01 09:07:07 2002 Page 2

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