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GCMS scan data for sample AE10812, May 2002

Machine-extracted title · confidence 100%

Fragmented GCMS scan data page showing tentative identification of compounds and surrogate recovery for sample AE10812.

NYC-WTC_000025533–000025541

Folder label: “GCMS X 5/17/02 A 5/16/02

Page image
Scanned page image, NYC-WTC_000025540
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY1302\10812.D Vial: 9 Acq On : 13 May 2002 11:42 pm Operator: Sample : GC/MS SCAN 5/7 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.68 0.49 ug/1 50381 Phenanthrene-dl0 25.54 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-d10 188 C14D10 001517-22-2 (87 2 Anthracene-dlO- 188 C14D10 001719-06-8 3 4H-Pyrido[1,2-a]pyrimidin-4-one. 3- 188 C11H12N2O 057773-19-0 40 4 2-Quin inecarboxaldehyde,8-hydrox188C10H8N202 005603-22-5 33 Abundance / Scan 2252 (25.680 min): 10812.D (-) m/z 188.15 100.00% KB

5000 ----- 80 94 42 54 66 158 25.40 25.60 25.80 26.00 PPTTT — — F"""11’ >>. 1.... 1.... 1 r 1 I— 11111 . Ill . m/z 94.10 16.11% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 KB

5000 25.40 25.60 25.80 26.00 m/Z 189.15 16.01% 80 160

m/z-> ....... 66... 11 ''' I'' ■1111111 11111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .. Ill. Abundance #19957: Anthracene-d10- KB 10 25.40 25.60 25.80 26.00 5000 m/ z 80.10 15.53%

. 80 94

mlz-> Abundance ' ‘ i ■" ‘ i ‘ 66 1 - rr i ! - 1’1:1117117111111111110111717 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 . l. #19873:4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- 145 KB 25.40 25.60 25.80 26.00 173 m/z 184.15 10.28% 92 5000

65 159 1111 " 111 ' "I' 'L i1" 11'' "i 1........ 119 132 | ।111' 11 11" 11 — ITT -------------- m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25,40 25,60 25,80 26.00

10812.D GCMS0510.M Tue May 28 14:26:40 2002 Page 3

NYC-WTC_000025540

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NYC-WTC_000025540Source: NYC Law Department, mirrored locally

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