GCMS analysis results, sample AE04944, April 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR3002\4944.D Vial: 11 Acq On 30 Mar 2002 12:52 am Operator: Sample gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title . : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyciopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 1.91 ug/1 306275 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 N-(Trifluofoacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 38 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 _4 PhenethylAmine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 'Abundance ' Scan 1068 (14.847 min): 4944.b(-) I m/z 73”7m 100.00% 73

5000 267 355

45 108 154 193 223 , 14.60 14.80 15.00 15.20 323' \..................................................... ' ' I ’ ' m/z 267.00 46.41% m/?:;?....... ; ...50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyciopentasiloxane, decamethyi- 713

■ 5000 267 355

14.60 i\ 14.80 15.00 15.20 m/z 355.05 44.15% , 207^ 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60152: N- ■if’uoroacety')-N O.d'.O' -tetrakisftnrsicihylsi 73 ..... . M , , , , , , 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 16.48%

45 I I 147 193 267 ........................ 538 , , rn/’z-> ____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis((trimethyTsilyl)oxy]-, trimet 73 14.60 14.80 15.00 15.20 m/z 268.00 12.12% 5000 355 45 j.......... 133 , . 193 223 281 H . m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

4944.D GCMS0308.M Tue Apr 02 11:07:37 2002 Page 1

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