GCMS calibration data for method 508, April 23 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.

NYC-WTC_000044313–000044337

Folder label: “GCMS X 4/23/02 A 4/26/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Phenol, 4-(1,1,3,3-tetramethyl Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

24.23 0.28 ug/1 52653 Phenanthrene-dl0 25.59

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 Phenol, 4-(1,1,3,3-tetramethylbutyl 206 C14H220 000140-66-9 78 2 Phenol, 4-(2,2,3,3-tetramethylbutyl 2 06 C14H220 054932-78-4 78 3 Phenol, chloro-4-(1,1-dimethylethyl 226 C12H15C1O2 055059-18-2.72 4 Tripyclo[4.3.1.13,8]undecane, 3-chl 184 C11H17C1 027011-47-8 43 Abundance Scan 2090 (24.230 min): 8757.D (-) m/z 135.00 100.00% 135

5000

41 . i.i ■ ' । 1 1 r’ 55 65 77 91 107 . I 121 | 1** '"I 1—711 1’1 )* 'I 1-1 r l | • ■ ■ ' | 1 > ■ 1 | ■ 1 1 ' | 1 ■ 1 ■ / 1 ' ■ 1 | —r 220 248 t t 1 ‘ I ' _AA 24.00 24.20 24.40 24.60 m/Z 107.00 12.37% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #70047: Phenol, 4-(1,1,3,3-tetramethylbutyl)- 135

5000 T I | I t rT [ I I I I | I I 1 I | I T"

24.00 24.20 24.40 24.60 m/z 136.00 10.42% 41 i 57 77 95 107 119 | 149 ——————————— " i 1 1 1 1 i 1 1 1 ' i ' ' ' ' i ' ' 1 1 i 1 1 1 1 i ‘ ' 206 1 ■ i ' ' m/z->_____ 40 60 80 100 1 20 140 160 180 200 220 240 Abundance #24409: Phenol, 4-(2,2,3,3-tetramethylbutyl)- 135 ■ 1 । 1 1 24.00 24.20 24.40 24.60 A_A 5000 m/ z 41.00 6.39%

miz-> Abundance 41

40 57

60 77 95 Y 119 80 ' 100 107

120 | T । i i i । I—r । i । । 140 149

AM160 #29051: Phenol, chloro-4-(1,1 -dimethylethyl)-, acetate 135 180 * । । । । 1 200 206 ।' । |" 1 1 220 i । । । 240

24.00 24.20 24.40 24.60 m/z 121.05 W 5.62%

NW 5000

150 — 107 211 22 49 95 । 119 .. ....... 226. I | > i - I —I—|—r- r . I | r ■ i > [-1 II ! | l) ’ I | > I V m/z—> 40 60 80 100 120 140 160 180 200 220 240 24.00 24.20 24.40 24.60

8757.D GCMS0412.M Tue Apr 23 08:22:56 2002 Page 4

NYC-WTC_000044322

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000044322Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

TCLP calibration table review document, April 2002 · Box DEP Box 25

NYC-WTC_000043238

Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.

1 shared topics · Same agency, volume and box · similarity 0.991