GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2 202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Silane, chlorotripropyl- Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

24.33 0.29 ug/1 53702 Phenanthrene-dl0 25.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, chlorotripropyl- 192 C9H21ClSi 000995-25-5 72 2 Phenol,/nonyl- 220 C15H240 025154-52-3 64 3 Phenol,/ 2-methyl-4- (1,1,3,3 -tetrame 220 C15H240 002219-84-3 43 4 2-Methyl-6-tert-octylphenol_________ 220 C15H24O 000000-00-0 38 Abundance Scan 2101 (24.331 min): 8757.D (-) m/z 149.00 100.00% 149 107 121 5000 191 1 1 1 1 1 i 411 55 77 91 134 220 24.00 24.20 24.40 24.60 1,11 I I , iL ।, ।lii 65 •1 I ,। iill I iili I* ! l. li T [ I I I r| rl r I | I I" ! | I ri i | i I r r| I I I I | I I ! I p i 1 I | i i । । I I । । । | । HTT | i i i i | i i i i | i i । 1 | i i j i | i i i i | i i i > | । । । । [ । । i > | ' > nq m/z 107.00 77.49% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 200 210 220 Abundance #20645: Silane, chlorotripropyl- 149 79 107 121 5000 i I | i i Ti | I 11 I | I I I I | I I I I |

24.00 24.20 24.40 24.60 m/z 121.05 53.30% 93 192 r'" i | I < I I | , I , I | I I ! I । I I > , | I ! I I | I I I । | I I TTTTTTTTTT r1" i * ’" i TTT I P , , | I ! I ! | ! ! ! i n rr) m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #27723: Phenol, nonyl- 149 107 1 I I I I I I I I I I I I I I I I I 1 1 i ■ ‘ 24.00 24.20 24.40 24.60 5000 m/z 191.10 28.66%

121 77 91 133 m/z-> I" " I " " I I i . i" " i" " i " " i I1....... ‘ITT P 161 ^177^ f1 ■" i" " i 30 40 50 60 70 80 90 100110120130140150160170180190 200210220 220 + Abundance #27697: Phenol, 2-methyl-4-(1,1,3,3-tetramethylbutyl)- 1 r । i i I-1 | l l r pl T 11 A । I । । i । 149 24.00 24.20 24.40 24.60 m/z 150.10 13.05%

5000

57 77 91 109 121 133 . 220 39 205 | TTTTTT 1111 _ J t _ . ■ 1............1............ 1........... I I I I I I 1 I I 1 I I I ■ I I I ■ I I I ■ 1 I I I I I I I I I I I I I I I ■ I -1 I11" I' ‘" I i1111111" i1 ‘" i11" I " 111 1 ' I ‘ ' TPEId ’ I ' > > ’l I m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 24.00 24.20 24.40 24.60

8757 .D GCMS0412.M Tue Apr 23 08:22:57 2002 Page 5

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