Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR22O2\8757. D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K. L Peak Number 6 Phenol, nonyl- Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T. 24.43 0.34 ug/1 62794 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenol, nonyl- 220 C15H240 025154-52-3 95 2 4-Nonylphenol 22 0 C15H240 000104-40-5 60 3 2-Nonylphenol 220 C15H240 000136-83-4 50 4 Tricyclo[4.3.1.13,8]undecane, 3-chl 184 C11H17C1 027011-47-8 45 Abundance / Scan 2112 (24.432 min): 8757.D (-) m/Z 135.00 100.00% 135 149 107 121 5000
I 41 55i 65 77 91 191 220 ALAA 24.20 24.40 24.60 24.80 1
m/z-> 1111II" ’ TI‘ 1 , 65, . . ... _ ., 4 I"'11 I + । ■ 1'" " । I | ill I | I I I I | | | I r | Il l ‘i ill i'1" i11" I 30 40 50 60 70 80 90 100110120130140150160170 180190 200 210220 m/ z 149.00 75.41%
Abundance #70560: Phenol, nonyl- 135
5000 107 121 149 1 1 I ' ' 24.20 24.40 24.60 24.80 m/z 121.00 56.52% 77 95 163 177 191 220,
WANu I TTTTTT0UTTTETTUITT r'" i T’T TWTBg——ngrr I''1 j m/z-> 30 40 50 60 70 80 90 100110120130140150160170 180190200 210 220 Abundance #70559: 4-Nonylphenol 135
24.20 24.40 24.60 24.80 5000 m/z 107.00 55.38% 107 121 149
163 177 191 220 i " " i " '' i 95 TTT 1———+ TH I" " I i" " i"''' i11" i" " i" " r "' I" " iH m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200 210 220 Abundance #27708: 2-Nonylphenol I I I I ■ I I I kl I I I I I I I I I I 135 24.20 24.40 24.60 24.80 m/z 91.00 16.38% 107 5000- 121
149 220 43 191 I 57 77 91 163 miz i1" 'i I I I I 1 1 I 1 I I I I I I I I I ll I ) I I I + 11" 11 । 1111" 1**0 i" " i’" " r "' i 30 40 50 60 70 80 90 100110120 130140 150 160 170 180190 200 210 220 24.20 24.40 24.60 24.80
8757 .D GCMS0412.M Tue Apr 23 08:22:58 2002 Page 6
NYC-WTC_000044324
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder