Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\APR22 02 \8757.D Vial : 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 7 Silane, chlorotripropyl- Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
24.52 0.27 ug/1 51483 Phenanthrene-dl0 25.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, chrotripropy1- 192 C9H21ClSi 000995-25-5 47 2 Phenol, nonyl- 220 C15H240 025154-52-3 43 3 4-Methyl'-2-t-octylphenol 220 C15H240 000000-00-0 35 4 Phenol,/ 2-methyl-4- (1,1,3,3 -tetrame 220 C15H240 002219-84-3 30 Abundance Scan 2121 (24.515 min): 8757.D (-) m/z 149.00 100.00% 121 149
MJ 107 5000
91 191 1 ' i ‘ 1 WV TTn—UT 39 55 65 -rj .. 111677 H r " 11" ■ ■ i ■1'' 11" 'I' ■ ■11 II 11 11" 11'" . 135 X 24.20 24.40 24.60 24.80 m/z 121.00 99.04%
MuL m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #20645: Silane, chlorotripropyl- 149 79 107
121 5000 24.20 24.40 24.60 24.80 m/z 106.95 63.24% 93 I l iff I I I I I j I I I I I > I I I I ।IIII|I!!!|!II।| pl I I [ I I I I I 1. 192 II I I I I I I I I I I I I I I I I t I I I I I A 11" " i" " i"'11 m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #70561: Phenol, nonyl- 121 1 ( । r । । । । । i । i |"
107 24.20 24.40 24.60 24.80 5000 135 m/z 191.00 17.63% N 163 77 91 177 149
m/z-> _________ i I . m ! ! I | ! 'I I ! | ! > I J| I ! ! ! | I I I I r | 1 I I I | I i < i"| i iTI p < i i | I i ’ H fill | i II I | I I i
30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 220 1" 11" " r ■" i 220 r1" r • "'i
Abundance #27675: 4-Methyl-2-t-octylphenol N TT 149 24.20 24.40 24.60 24.80 m/z 91.00 16.18%
5000 121 57 ...................| 91 220 1’11111011117711 ........... I..... r " 1 r1" i ■" ■ i 1994— 133 i ’ 11 *TO H mfe-> 30 40 50 60 70 80 90 100110 120130140 150160 170180190 200 210 220
8757.D GCMS0412.M Tue Apr 23 08:23:00 2002 Page 7
NYC-WTC_000044325
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder