Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Phenol, 4-(1,1,3,3-tetramethyl Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
24.64 0.27 ug/1 51078 Phenanthrene-dl0 25.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenol, 4- (1,1,3,3 -tetramethylbutyl 206 C14H220 000140-66-9 59 2 Phenol, /4 - (2,2,3,3-tetramethylbutyl 206 C14H220 054932-78-4 45 3 Phenol/ 4-(2,2,4-trimethylpentyl)- 206 C14H220 000000-00-0 40 4 4-Nonylphenol 22 0 C15H240 000104-40-5 34 Abundance Scan 2135 (24.644 min): 8757.D (-) m/z 135.00 100.00% 135
5000-
m/z-> 41 1 55 65 77 'l " 1 1 - i f . r‘4 i | । i i » j . i Pi | 95 । fvdns 107 121 ' _____ j______ 1 I I I I I I I I I 1 I I I I I I
30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 220 '1 r 147 163 177 r ■111'''1 ■ i11''' r i" " i" " i 220 "i" "’i W) m/z 107.00 24.40 24.60 24.80 25.00 20.52% Abundance #24424: Phenol, 4-(1,1,3,3-tetramethylbutyl)- A 135
5000 24.40 24.60 24.80 25.00 m/z 135.95 11.01% 57 107 39... | r1" i1" 1 r1111 95 | ng 77 l'" '' I ftp rr’r11 1.150 i ■ *" i11" i" " i TTTTT 206 I "111" " 11" 11 m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #24409: Phenol, 4-(2,2,3,3-tetramethylbutyl)- 135 j —AA 24.40 24.60 24.80 25.00 5000 m/z 41.05 10.06%
m/z-> Abundance 41 । 57 I ।"1111 i'(" i i " 77 95 107 ( 119 r NTT A 11111111111'| 11 149 1 r 1 11 110 r " 11"1111" ‘I 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 220 206 [ i i I'i । । i ' | I i i i |
#24397: Phenol, 4-(2,2,4-trimethylpentyl)- 135 i i
/Aw W 1 ' 1 ' 1 1 1 ' 1 I 1 1 1 1 1 1 24.40 24.60 24.80 25.00 m/z 121.00 7.39%
5000
57 I 77 91 107
160 206 ANW. i11" i'1" i"111 i11 "Ir Mo ' i'r I i " I " " i " P 1 ‘T i" 11 r 111 i 11 I i i i । r i i i l 1 I I | I r i i । i i
m/z—> 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 220 24.40 24.60 24.80 25.00
8757.D GCMS0412.M Tue Apr 23 08:23:01 2002 Page 8
NYC-WTC_000044326
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
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NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
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NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
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NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder