Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Phenol, nonyl- Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
24.77 0.31 ug/1 57441 Phenanthrene-dl0 25.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenol, nonyl- 220 C15H240 025154-52-3 (93 2 Phenol, 2-methyl-4-(1,1,3,3-tetrame 22 0 C15H240 002219-84-3 52 3 4-Methyl-2-t-octylphenol 220 C15H240 000000-00-0 38 4 Nitrofurantoin 238 C8H6N4O5 __ _______ 000067-20-9 36 Abundance Scan 2149 (24.772 min): 8757. D (-) m/z 149.10 100.00% 149
107 5000 121 177 ) W V, , . 24.40 24.60 24.80 25.00 25.20
m/z-> 41 55 65 77 91 -T , H 133 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 A 220 TWTTITTTTTTTT] m/z 107.00 58.31% Abundance #27723: Phenol, nonyl- 149 107
----- ——1—A4—1—1 1 1 1 '—1—1—1—1—A-p—4 5000 24 40 24.60 24.80 25.00 25.20 121 m/z 121.05 25.45% 77 91 11 - " । I I . । " i"1' i" " i " " t ...... ...... 133 ..161., 177, 220 TCIUTT
MWLA m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #70548: Phenol, 2-methyl-4-(1,1,3,3-tetramethylbutyl)- 149 1 ' i ' 24.40 24.60 24.80 25.00 25.20 5000 m/z 177.05 17.74%
121 91 109 133 220 TTTTTETTat 164 ........ I P I " " I " " I " " i" 111" " i m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #27675: 4-Methyl-2-t-octylphenol T-T 1I ........ A. ’ ' ' 1 1 1 1 ‘ ‘ 1 1 149 24.40 24.60 24.80 25.00 25.20 m/ Z 150.00 12.09%
5000 121 57 91 1 -++ 109, r 1" i" " I " " I 133 11" " i TTT 111111 220 HH m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 24.40 24.60 24.80 25.00 25.20
8757.D GCMS0412.M Tue Apr 23 08:23:02 2002 Page 9
NYC-WTC_000044327
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder