Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\ 1\DATA\APR2 202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Phenol, 4-(1,1,3,3-tetramethyl Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
24.87 0.34 ug/1 64464 Phenanthrene-dl0 25.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenol, 4-(1,1,3,3-tetramethylbutyl 206 C14H220 000140-66-9 78 2 Phenol / 4 -(2,2,3,3-tetramethylbutyl 206 C14H220 054932-78-4 78 3 Butane', 1,3-dibromo- 214 C4H8Br2 000107-80-2 43 4 Phenol, 2-methyl-5-(I-methylethyl) - 150 C10H140 000499-75-2 43 Abundance - Scan 2160 (24.873 min): 8757.D (-) m/z 135.00 100.00% 135
5000 W. 107 24.60 24.80 25.00 25.20 41 ..... | l"" P 55 65 77 86,95 | 121 । i i'i i | i iT i p i i i । i i i i । I । i i । i ill | i r i i | । i i > | 1,149 । i i i i । i । A | i i i i | 220 i" " i TTTTT m/z 107.00 13.24% m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #70047: Phenol, 4-(1,1,3,3-tetramethylbutyl)- A A 135
V 5000 i ' 1 ' ' i 24.60 24.80 25.00 25.20 m/ Z 136.00 12.36% 41 77 57 95 107 119 206 ___ L_ 1 | 149 I"111' TTTTuOmouuiut 11 r 1111" r H ■ i" 111" " i i'1" i । i-! It । 111 । । । । । ।
m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #24409: Phenol, 4-(2,2,3,3-tetramethylbutyl)- 135 AlY.......... । । । I । i I । । i । ■ । । r
2460 24.80 25.00 25.20 5000 m/ z 41.05 8.01%
m/z-> Abundance 41 i 57 77 95 107 119 L TWTPWTpunooaf i •" "T’III ‘ITT 206 " r1" r1" i"'11" H i"111" " i 30 40 50 60 70 80 90 100110 120130140150160170180190 200 210 220
55 #70305: Butane, 1,3-dibromo- 4149 135 W ’ ' 1 1 1 1 1 1 1 ' 24.60 24.80 25.00 25.20 WMW m/ z 91.00 4.28%
5000
216 107
m/z-> r 11' i " " i ........... 95 i" " r " 11 ■ ■" i ’1 “i1 30 40 50 60 70 80 90 100110 120130140150160 170180190 200210 220 II 121,1.... I''" I " " I " " I •... I—— Ai - 24.60 24.80 25.00 25.20
8757.D GCMS0412.M Tue Apr 23 08:23:03 2002 Page 10
NYC-WTC_000044328
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
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Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
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Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
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