Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L Peak Number 11 Phenol, nonyl- Concentration Rank 18
R.T. EstConc Area Relative to ISTD R.T. 25.02 0.21 ug/1 38994 Phenanthrene-dl0 25.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenol, nonyl 220 C15H240 025154-52-3 52 2 Phenol, 4-(l, 1-dimethylethyl) -2-met 164 C11H160 000098-27-1 50 3 Phenol, 2-methyl-4-(1,1,3,3-tetrame 220 C15H24O 002219-84-3 40 4 Tricyclp.-{4.3.1.13,8] undecane, 1-bro 22 8 CHH17Br _______021898-96-4 33 Abundance Scan 2176 (25.020 min): 8757.D (-) m/z 149.00 100.00% 149
5000 107
121 I 1 I I I W. I I
24.60 24.80 25.00 25.20 25.40 I I 1 I 17/15 ri 10 fi’t 39 55 65 77 91, | 133 — i"111"11 r ‘" i 220 m/z 107.00 41.29% r " I’u’ 111 ih i11" "'i" " i'"'" i I......-I1.. . । | iH , , । "I..... m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance
5000 #27723: Phenol, nonyl- 107
121 149
MM I ' ' ' ' I 1 1 ' ' 1 1 ' 24.60 24.80 25.00 25.20 25.40 m/z 121.05 I TIl
13.68% 77 91 I I . i" " i" " i" " i" " i" " i" " i " " i 133 TT 220 ..161., 177 I" " I " " I 11 r " r i m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200210 220 Abundance #13553: Phenol, 4-(1,1-dimethylethyl)-2-methyl- 149 WW.. 24.60 24.80 25.00 25.20 25.40 5000 m/z 150.00 11.60% 164 . 121
l'1" i" '11" HI 7791.. 199.1133 i" " r " ’T’ H11" "i1" ‘ i ■ ■ ■11'1'11'1 m/z-> _ 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 I'"' I" " I'" ‘ I" '' I" " I
Abundance #27697: Phenol, 2-methyl-4-(1,1,3,3-tetramethylbutyl)- 149 24.60 24.80 25.00 25.20 25.40
5000
m/z—> 39 57 i" "i 111111 Tl 91 I . I 109 121 133 , . I O——B00"T111"111011111 —0000—I 010137TT I 205 220 I‘ II‘‘IINII" ‘' 11" ‘ I 30 40 50 60 70 80 90 100110120130 140150160170 180190 200 210 220 yw m/z
TTT 54.95
24.60 24.80 25.00 25.20 25.40 10.40%
8757.D GCMS0412.M Tue Apr 23 08:23:04 2002 Page 11
NYC-WTC_000044329
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
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NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
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NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder