GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR2 202\8757.D Vial: 13 Acq On 22 Apr 2002 8:55 pm Operator: Sample gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Anthracene, 2-methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

25.23 0.29 ug/1 54392 Phenanthrene-dl0 25.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 50 2 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 43 3 Phenanthrene , 1-methyl- 192 C15H12 000832-69-9 43 4 Phenanthrene, 2-methyl - 192 C15H12 002531-84-2 43 Abundance Scan 2199 (25.231 min): 8757. D (-) m/z 192.00 100.00% 192

5000 266

60 71 82 96 107118 130 146 160 25.00 25.20 25.40 25.60

m/z-> 41 iitphtii 40 60 80 100 , Il 1 II,....... 11 120 140 I I I

160 I I I I I

180 I I ’ 1294. 230 ■ i' 200 220 240 ' i " 260 m/z 265.80 29.31% Abundance #69327: Anthracene, 2-methyl- 192

/ 5000 iUt 25.00 25.20 25.40 25.60 m/z 191.10 23.35% 96 165. ■ । ■ ■ ■ ■ । 176 ■ 1 I i > ■ ..................152 | । । I- । ‘i 1 1 ' i ' । i [i-n-i-| ’ ’II T ■ i 1 ' 1 1 I ■ ■ ' 1 i ' ' ' ■ i 1 ■ m/z-> 40 60 80 100 120 180 200 140 160 220 240 260 Abundance #20870: Phenanthrene, 3-methyl- 192 A 25.00 25.20 25.40 25.60 5000 m/z 2 67.80 17.97%

96 139 152 165176 1 1 1 i 1 1 1 1 i ' ■ । > ■ ■ । । ■ ■ ■ ■ । ■ mlz—>_____ 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #69330: Phenanthrene, 1-methyl- 1 ' i 1 1 ‘ 1 ' I ' 1 ' ' i 1 1 192 25.00 25.20 25.40 25.60 m/ z 193.00 17.04%

5000

..... J..... 152 165 178 1 ' 1 1 i I ! | I I I । [ । i i । [ I I ri ] 1 i i r | I i i i | “I i I i | i i i I । i i i 1 । । । । । । । । "I I-1 I I I I I I I I I I I I I I I T 1

n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 25.00 25.20 25.40 25.60

8757.D GCMS0412.M Tue Apr 23 08:23:05 2002 Page 12

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