Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
NYC-WTC_000046249–000046265Folder label: “GCMS X 5/7/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAY0302\9579.D Vial: 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 2-Hexenal Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
20.67 2.38 ug/1 201649 Acenaphthene-dl0 21.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Hexenal/ 98 C6H10O 000505-57-7 30 2 Cyclopenbane, 1,1,3,4-tetramethyl-, 126 C9H18 020309-77-7 22 3 Cyclopropane, 1,1,2,2-tetramethyl- 98 C7H14 004127-47-3 10 4 Cyclopentanepropanoic acid 142 C8H14O2 000140-77-2 10 Abundance / Scan 1705 (20.665 min): 9579.D (-) m/z 55.10 100.00% 41 55 73
83 5000 111 10 ( I i f f i i r J | 1 i i I ’ |- i i 98
m/z-> 1 ■ 11 11 11 ■ ‘1 ■ l ’ Illli . " 10 20 30 40 50 ilaesl —+ 90_+++LHH 60 70 80 129136 144 154 100 110 120_1301401 50 160 7 | n I r i i I i | I I I I | I I I I | | I m/ Z 20.40 20.60 20.80 21.00 73.10 86.45% Abundance #63218: 2-Hexenal 31 42 55 69 83 7 / 5000 20.40 20.60 20.80 21.00 98 m/z 41.15 83.85%
m/z-> 10 20 30 "II 1111... .... । 11 11 r 11 1 i1 11 1 r 1 11 ।1 11 11 40 50 60 70 80 90 100 110 120 130 140 150 160 T’’ Abundance #64931: Cyclopentane, 1,1,3,4-tetramethyl-, trans- 69 83 41 55 111 20 40 20.60 20.80 21.00 5000 m/ z 60.00 63.50%
95 I!11 1 I ■ ■1 11 ■ ■ ■ ■ l ■ • ■ ■ [ ■1 ■1 I TT3 TTT ■1 1 i m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #1363: Cyclopropane, 1,1,2,2-tetramethyl- YAA 55 20.40 20.60 20.80 21.00 83 m/z 43.05 54.21% 41 5000 ) 27 98
m/z-> 15 | ■ । ■ ■ - ■ । ■ 1 ' i ■ 10 20 30 1 i11 ’ 11 1 40 50 L ‘ 1’’ 1 1 1 1 ‘ ' I ‘ 60 70 80 90 100 110 120 130 140 150 160 1’11’11111111111112111117 20.40 20.60 20.80 21 00
9579.D GCMS0501.M Mon May 06 10:49:56 2002 Page 9
NYC-WTC_000046262
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024997
Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000046213
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 7-9 2002.
Filed in the same folder
NYC-WTC_000046214
Single page excerpt from a GCMS laboratory record file stored in DEP Box 25, dated between May 7 and May 9, 2002.
Filed in the same folder
NYC-WTC_000046217
Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
Filed in the same folder
NYC-WTC_000046226
Laboratory report of GCMS calibration analysis for sample AE09579 conducted on May 8, 2002, listing detection limits.
Filed in the same folder
NYC-WTC_000046230
Laboratory report of GCMS reference analysis for sample AE09579 conducted on May 8, 2002, showing response factors.
Filed in the same folder