GCMS analysis results for sample AE01498, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1498.D Vial: 21 Acq On : 22 Feb 2002 11:46 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentane, 1-ethyl-2-methyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.76 0.32 ug/1 25204 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentane/ 1-ethyl-2-methyl-, ci 112 C8H16 000930-89-2 43 2 2-Heptenal ,/(E)- 112 C7H120 018829-55-5 38 3 1-Heptanol/ 6-methyl- 130 C8H180 001653-40-3 38 4 Isooctanoi 130 C8H180 026952-21-6 38 Abundance Scan 2039 (23.763 min): 1498.D (-) | m/z 55.0,0 100.00% 43 55 69 83

97 5000 111 —A m/z-> " r"'r"11"" r"' I Imp m 23.40 23.60 23.80 24.00 1 ■ i'11 'i" " Ji" " i ■1 m/ z 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 1" i" " r 43.0.5 91.60% Abundance #2670: Cyclopentane, i-ethyi-2-methyl-, cis- i 55 83 41

5000- 70 । ’ I* A 27 23.40 23.60 23.80 24.00 m/z 41.05 88.57% 97 112 " i“ " । ■ TTTTTTTTTTTTTTTTTTTTTTTTITTTTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance "034 ■ 27 55 83 39 TT ..... A..... I 1 ' ■ ' 1 1 ' 1 1 1 1 23.40 23.60 23.80 24.00 70 5000 m/ z 69.1.0 88.32%

97 112 1' ‘ i ■" ‘ r ■" i"" r " ■ i" " i" " I" "I" ■ ■ r ■" r "11" " i ■ ■ ■' i'" ‘ i" " i" " r "' r'11 r "' i'" ‘ r'" i" {m/z->____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #65310: 1-Heptanol, 6-methyl- 11 ■ ■ ■ ■ । ' ■ ‘ । ‘ ।1 55 69 23.40 23.60 23.80 24.00 m/ Z 83.0.5 86.47% 5000 84

27 42 97

m/z-> »* 11' l * I •«> *) ’ TIIUE011111 TTp-rrq-m- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Ip I ■1,11' ■" i' ।" r " 'i “ " i" "i" " i" 23.40 23.60 23.80 24.00

1498.D GCMS0208.M Tue Feb 26 15:08:11 2002 Page 3

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