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GCMS analysis results for sample AE01498, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01498 conducted on March 6, 2002.

NYC-WTC_000003628–000003638

Folder label: “GCMS X 1/23/02 A 2/22/02

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Scanned page image, NYC-WTC_000003636
OCR text

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\1498.D Vial: 21 Acq On : 22 Feb 2002 11:46 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1-Dodecanol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

20.72 0.61 ug/1 53543 Acenaphthene-dl0 21.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

( 1-Dodecanol 186 C12H260 000112-53-8 91 21- Unde c anol 172 C11H240 000112-42-5 91 3 Cyclotet radecane 196 C14H28 000295-17-0 68 4 1-Decene 140 C10H20 000872-05-9 64 Abundance Scan 1708 (20.725 min): 1498.D (-) m/z. 55.00..100.00% 43 55 69 ! 83

5000 97 - 111

m/z-> m4 ...... I ,| I, 125 140 ' p'11 ■ ■■11111 ■ ■ i1111 p11' i'' " p " ■ p • ■ ■ l' ‘' ■ p' " p ' ‘' p "' p ■ ■' p " ‘ p1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.40 20.60 20.80 21.00 m/z 43.05 85.90% Abundance #69118: 1-Dodecanol 55 69 83 / n 5000- 97 20.40 20.60 20.80 21.00 42 | 111 m/z 41.05 85.84% || li 125 140 । p ■ । । । ■11 TTIWHIOTTTRTTTITTIWTIIWITPTTT m/z->:20 30 40 50 TIUI " p ■ i ■* p 60 70 80 90 100 110 120 130 140 1 50 160 170 180 190 200 Abundance 55 69 83 TI w ’ i ■ 1 ' ■ i 20.40 20.60 20.80 21.00 5000 97 m/z 69.00 79.45% 42 111 126

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 - Abundance #69524: Cyclotetradecane 55 20.40 20.60 20.80 21.00 m/ z 83.05 66.85% 83 5000 70 97 27 42 111 | 125 ' p' “ p' " i 11 p ■ 11′8 '" ■ i -THr ' p1" p "' p ■ ■ ■ i'' " p "168 196 ' p “' i' “ ' p '1 ■ p ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.40 20.60 20.80 21.00

1498.D GCMS0208.M Tue Feb 26 15:08:07 2002 Page 2

NYC-WTC_000003636

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NYC-WTC_000003636Source: NYC Law Department, mirrored locally

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