GCMS blank analysis report, May 6, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 6 02\LB.D Vial: 3 Acq On 6 May 2002 11:27 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 1-Dodecanamine, N,N-dimethyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

26.62 1.08 ug/1 99331 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Dodecanamine, N,N-dimethyl- 213 C14H31N 000112-18-5 64 2 N, N-Dimethyloctylamine 157 C10H23N 007378-99-6 64 3 1-Dimethylaminohexane 129 C8H19N 004385-04-0 43 4 2-Butanol,/1-(dimethylamino) -_____ 117 C6H15NO 003760-96-1 43 Abundance 7 Scan 2355 (26.623 min): LB.D (-) m/z 58.10 100.00% 58 ft 5000 ) i 1 ■ 11 i 1 1 1 n 1‘‘I‘ 41 26.20 26.40 26.60 26.80 27.00 84 188 269 oV - * .I | i 71 r' i T | 1 1 i | > i i i |~"i~'|_| I | i i i i । i i i < । i 1 i I | > i i i j f-! i i । । | । i । i i i i m/z 41.05 4.87% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #26133: 1-Dodecanamine, N,N-dimethyl- 53

5000 A 26.20 26.40 26.60 26.80 27.00 m/z 43.15 4.49% 42 84 114 156 170 184 198 213 i 1 1 1 ' i 1 1 A ' ' 1 1 1 1 ' ' 1 1 1 1 1 ' I ' ' ' 1 | ‘ ' | 1 1 1 1 I 1 1 1 rT 1 1 1 ' 1 1 1 1 1 I 1 1 1 1 1 1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #11740: N.N-Dimethyloctylamine 53 N-PPM 26.20 26.40 26.60 26.80 27.00 5000 m/ Z 59.10 3.96%

30 42 1 , I 11 ■ , .11 I ' ' ' ' 1 1 ' ' , , ' i ■ ■ ■ 84 ■ i ' ' 114 157 ' 1 1 1 1 1 ' i ' ■ ' ■ I 1 ' ■ ■ i ' ' ' ' i ■ 1 ■ ■ i ' 1 ' ' i ■ ' ' 1 i 1 1 1 1 I ' 1 mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5271:1-Dimethylaminohexane i 1 ■ ■ 1 i 1 i ■ 1 ' ■ i ■ ' 53 26.20 26 40 26.60 26.80 27.00 m/ z 55.10 2.26% 5000

29 42 84 129 i 11"’ 1 i 1 ‘ 1 1 [ । । । । ] 1 । [ i i i । | r I । । | । । । । । । । । । । j i । । । i i i i ] । । । p ।—।—। । । । । A _ A / V /A A A A RVV j 1 ।। । I । ।। । | i । r । p I I r i । i r m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 26.20 26.40 26.60 26.80 27.00

LB.D GCMS0501.M Wed May 08 11:53:45 2002 Page 3

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