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Document / 13 pages

GCMS blank analysis report, May 6, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.

NYC-WTC_000043547–000043559

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0602\LB.D Vial: 3 Acq On 6 May 2002 11:27 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Morpholine, 4-[3-(trimethoxysi Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 26.49 3.00 ug/1 275589 Phenanthrene-dl0 25.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Morpholine, 4-[3-(trimethoxysilyl)p 249 C10H23NO4Si 031024-54-1 40 2 Furaltadone 324 C13H16N4O6 000139-91-3 39 3 Butanamide, 2 - (dimethylamino)-N-[7 - 593 C35H39N5O4 018397-13-2 39 4 4 -Morpholineethanamine 130 C6H14N20 002038-03-1 9 Abundance Scan 2340 (26.486 min): LB.D (-) m/z 100.10 100.00% 100

5000

....... ) ' ' I > ' 1 I I I ' • I TUl I I I I I \1 70 ■ 26.20 26.40 26.60 26.80 126156 210 255 > । > | 1 I I t ] 1 I I- ! [ I I < i 1 1 1 । | 1 । 7 1 । I । I | > I I I | I I I 1 | I I I Cgt m/z 41.10 5.99% m/z-> 50 100I 150 200 250 300 350 400 450 500 550 600 Abundance #33645: Morpholine, 4-[3-(trimethoxysilyl)propyl]- 100

..................... ....................... 5000 26.20 26.40 26.60 26.80 m/z 101.15 5.78% 56 1 131 162 f ' 1 i 1 1 1 ' i 223249 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #46033: Furaltadone 100

26.20 26.40 26.60 26.80 5000 m/ Z 43.05 5.48%

56 128 185 j i 1 ■ 1 i 1 T • > ' • । ‘ । i i । । । । । | । i । । l i i i । । "r i i । i i i i । । i"r i । i i i i । i i । ।— v /z->____ 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #60761: Butanamide, 2-(dimethylamino)-N-[7-(1H-indol-3-ylme A Mal * -IMP9n 100 26.20 26.40 26.60 26.80 m/ z 42.05 4.40%|

5000

130

n/z-> 42 70 TIr-t 50 I 170 T'l Pl | I I I

100 150 224 'I..... . ■ । । 200 250 300 । । । 350 । 400 । 550 593 । . . . . । . . . . [ । । । । । । 450 500 550 600 -A 26.20 26.40 26.60 26.80

LB.D GCMS0501.M Wed May 08 11:53:44 2002 Page 2

NYC-WTC_000043554

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NYC-WTC_000043554Source: NYC Law Department, mirrored locally

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