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GCMS sample AE07106 analysis report with surrogate recovery, Apr 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.

NYC-WTC_000043458–000043471

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1802\7106.D Vial: 25 Acq On : 19 Apr 2002 11:38 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 2,6-Dimethyldecane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

14.99 0.49 ug/1 114823 Naphthalene-d8 15.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,6-Dimethyldecane 170 C12H26 013150-81-7(83 2 10-Methylnonadecane 282 C20H42 000000-00-0 58 3 1-Decanol, 2-ethyl- 186 C12H260 021078-65-9 53 4 Eicosane, 10-methyl-_____________ 296 C21H44 054833-23-7 53 Abundance Scan 1084 (14.995 min): 7106.D (-) m/z 57.00 100.00% 43 57

71 5000 85

112 | । i r i | i i i i । i I I I V j i i i i । i i

97 14.60 14.80 15.00 15.20 15.40 - 126 168 I | | | Ji T1u —l—uall — P111|1''1| — m/z 43.00 92.19% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #15357: 2,6-Dimethyldecane 43 57 71

5000 85 14.60 14.80 15.00 15.20 15.40 27 113 m/z 71.00 62.60%

m/z-> 20 30 40 ■ ■ j ■

50 TIT — 60 i. JU 70 80 90 100 110 120 130 140 150 160 170 I 1 1 ' ’ I 1 1 ' ' I 170 T

Abundance 57 #39858:10-Methylnonadecane

71 _WW 1 ' i 1 1 14.60 14.80 15.00 15.20 15.40 85 5000 m/z 41.05 48.82%

99 154

m/z-> 20 30 42

40 50 —l 60 +T --- 113 126 P '1 11 70 80 90 100 110 120 130 140 150 160 170 _NAMV "V WW Abundance #19527: 1-Decanol, 2-ethyl- I "Il j I I I I I l f l ) I I I I I I I1 I

43 57 14.60 14.80 15.00 15.20 15.40 m/z 85.05 40.83%

5000 71 83 4 | I | | I | I I I | | 1 I | | i r -1-p-T 97 I 444 111 126 168 _ AAAA/V V i । I । । । । । । । । । । । । । I । । । । । । । । । । । । । । r। । i i i i । । ' i । । । । r । । । i । r i [ > । m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 14.60 14.80 15.00 15.20 15.40

7106.D GCMS0419.M Mon Apr 22 08:34:01 2002 Page 5

NYC-WTC_000043467

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