GCMS sample AE07106 analysis report with surrogate recovery, Apr 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR1802\7106.D Vial: 25 Acq On 19 Apr 2002 11:38 am Operator: Sample GC/MS SCAN 3/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Undecane, 3,7-dimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

15.15 0.53 ug/1 124394 Naphthalene-d8 15.85

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

I Undecane, 3,7-dimethyl- 184 C13H28 017301-29-0 59 2 Decane/ 2,9-dimethyl- 170 C12H26 001002-17-1 59 3 Nonadecane 268 C19H40 000629-92-5 53 4 1-Undecene, 4-methyl-__________ 168 C12H24 074630-39-0 53 Abundance Scan 1101 (15.151 min): 7106.D (-) m/z 43.05 100.00% 43 57 ft 71 5000 85 _AW_A ' I ‘ ' 1 1 1 1 ‘ ' 1 1 1 ' 1 1 1 1 1 1 ' 1 1 97 126 14.80 15.00 15.20 15.40 l " 1 140|l q+ TTm 4---—r 1,1 113, 11155............... । I । । II । । ii । D I I n | i I i I | ! I I । | i । । । | । i 7 j I I i i | i r m/ z 57.00 89.31% m/z-> 20 60 80 100 120 140 160 180 200 220 240 260 ft ft Abundance #19002: Undecane, 3,7-dimethyl- 43 57

5000 71 85 W WW —————————— 14.80 15.00 15.20 15.40 ' ' i '

m/ Z 71.10 61.02% 27 1i ' ■ ■ ' i ' 1 i 1 1 U 99 113 127 155 n m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #15361: Decane, 2,9-dimethyl- 43 57 TT V 14.80 15.00 15.20 15.40 W/V/ ■ ■ I b

5000 71 m/ Z 41.00 46.70% 85 27 I m/z-> Abundance 20 i ■ ■ ■ • । 40 43 57 ■ I ' 1 ' ' 1 1 60 80 99 113 127 100 120 140 160 180 155

#71948: Nonadecane 200 220 240 260 JW WyN ' I ' 1 1 ■ 1 1 1 1 ‘I’’’‘I‘ 14.80 15.00 15.20 15.40 m/z 85.00 44.18% 71 N 5000 85

m/z-> l 1 ' ' ’ i ' 20 40 J TuB 60 80 99 !tl I । । ! [i । ri i i ] n m । r-! 11 | । 100 113 I 127 I

120 140 156 160 180 196 210 225 268 1 1 i 1 1 1 1 i 1 1 1 ' i ' 1 ■ 1 i 1 1 ■ 200 220 240 260 AAAWVU I j I I I I I II I I I I I I I I I I I I I I 14.80 15.00 15.20 15.40

7106.D GCMS0419.M Mon Apr 22 08:34:02 2002 Page 6

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