TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Undecane, 5-methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 15.01 0.25 ug/1 49180 Naphthalene-d8 15.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, 5-methyl- 170 C12H26 001632-70-8 43 2 Octane, 1,1' -oxybis- 242 C16H340 000629-82-3 38 3 Octane, 4-methyl- 128 C9H20 002216-34-4 37 4 Eicosane 282 C20H42 000112-95-8 37 Abundance Scan 1086 (15.013 min): 8481.D (-) m/z 57.00 100.00% / 43 57

5000 71 85

95 112 i 1 r 1 ' i ' 14.60 14.80 15.00 15.20 15.40 J.Li i I ] i i 1 l i i " f r-

i 1 1 1 1 T 41 ii ' i 1 I i 11 n | । । i । | t [ i l i ! i । i i l । l i f । i r m/z 4 3.05 84.69% m/z-> 20 40 60 80 100 120 140 160 180 200 220 A Abundance

N #68258: Undecane, 5-methyl- 43 57

71 5000 85 | I <1 L I i i i । । i i 1 । : i i i । i i 14,60 14.80 15.00 15.20 15.40 112 m/ Z 71.00 70.46%| 99 || 126 140 155 170 fl i ■ ■ > ■ i ■ ■ " i ' 1 1 ' i 11 । T। । I । [ i । । । । । । । ! | l i I"I r 'i i i [ v । i । । i fl

. A. m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #71251: Octane, 1,1’-oxybis- 57 71 \A U | । t 1 । j if n । i । । । । rm i i । i r

14.60 14.80 15.00 15.20 15.40 5000 m/z 41.05 60.11% 84 fl 112

m/z-> Abundance 20 i 40 42 — 60 1 i 80 97 ' 1 i 1 100 ■ i 120 #65131: Octane, 4-methyl- • ■ ■ ■ 140 143 i - i I

160 [ I I I I

180 | i । । i

200 | । 210 224 । i 1—i—r

220 MM VV 1 i ■ 1 1 1 i 1 1 43 14.60 14.80 15.00 15.20 15.40 m/ Z 85.05 55.72% | 5000

57 71 85 27 | TIT ,1 III. i ' 1 . . |....... 128 ___________ 1 | 1 fi 1 | l 1 । | । 1 ’ 1 [ । i । । | । 1 i । [ । । । 1 । । i—i—[—i—i—i—।—i—r \ /M | i । “ | “ if 1 \l. Y. "y vy ri f i ।—ri—i i |—kk m/z-> 20 40 60 80 100 120 140 160 180 200 220 14.60 14.80 15.00 15.20 15.40

8481.D GCMS0412.M Fri Apr 26 12:47:25 2002 Page 6

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