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GCMS analysis results for sample AE01441, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01441 analyzed via GCMS on March 6, 2002, including surrogate recovery data.

NYC-WTC_000009885–000009896

Folder label: “GCMS X 1/22/02 A 2/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\ FEB2 1021441.D Vial: 13 Acq On : 22 Feb 2002 1:55 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Undecene, 2,5-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.28 0.91 ug/1 53064 Perylene-d12 38.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Undecene, 2,5-dimethyl- 182 C13H26 049622-16-4 16 2 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 16 3 Octane, l,l/-oxybis- 242 C16H34O 000629-82-3 14 4 Propanedioic acid, hexyl-, diethyl 244 C13H24O4__ ____ 005398-10-7 12 Abundance.’.... /. ‘. . .Scan 3402 (36.277 min): 1441. D(-) ' “ m/z 185 .Tb 100.00% 185

57 5000 70 43 112 83 98 36.00 36.20 36.40 36.60 1 1 ' 1 ' T 1 ' ' ' 1 1 11 ■ 1 miz-2__ 20_ ............. 60__ 80 ' 'I 1 1 100120 140 143 .... 11 160 ...... 180 4298- 200 220 m/z 57.00 55.90% Abundance #18488: 2-Undecene, 2,5-dimethyl- 57 69 A 5000 36.00 36.20 36.40 36.60 m/z 70.00 42.92% 27 m/z->.. 20 i ■ * » * i 40 42 |■ * 60 -4 80 97 100 111 120 126 140 _ 1J0 180 182

200 220 Abundance dune 0 1 mem 09.60-(Z) ................................ 43 57 69 1‘I* 36.00 36.20 36.40 36.60 5000- m/z 71.00 38.29% 83 98 112

y_ 140 ................................................................ /................ i.......................... 182............................... m/z->___ 20 ...... 40........ 60___ 80 100 120 140 160__ 180 200___ 220 Abundance #71251: Octane, 1,1’-oxybis- ■ ■ i ■ ■ ■ ■ i 57 71 36.00 36.20 36.40 36.60 m/z 55.00 30.30% 5000 84 42 112 97 143 210 224 । ■ ■ ■ ■ i ■ • Iif ' i m/z-> 20 40 60 80 100 120 140 160 180 200 220 ___ 36.00 36.20 36.40 36.60

1441.D GCMS0208.M Fri Feb 22 09:35:56 2002 Page 4

NYC-WTC_000009895

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NYC-WTC_000009895Source: NYC Law Department, mirrored locally

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