GC/MS analysis report, sample AD23719, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23719.D Vial: 15 Acq On : 16 Oct 2001 1:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Undecene, 4,5-dimethyl-, [R@ Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 35.66 0.83 ug/1 79348 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm , CAS# Qual 1 2-Undecen^< 4,5-dimethyl-, [R@,S®-( 182-C13H26.? 055170-93-9. 25 2 1-Decen^< 2,4-dimethyl- 168 C12H24 055170-80-4 17 3 Prop 3edioic acid, hexyl-, diethyl 244 C13H24O4 005398-10-7 14 4 Naply halene, l-isothiocyanato- 185 C11H7NS . 000551-06-4 12 ^bundance Scan 3336 (35.663 min): 23719.D (-) m/z 185.10 100.00% Ite

253 43 57 71 112 ■1 Tife-> Abundance u T ............... . 125 30 40 50 60 70 80 90 100110120 130140 150160170180 190 200 210 220 #18485:2-Undecene, 4,5-dimethyl-, [R@,S@-(Z)l- .. ...... I m/z 35.40 35.60 35.80 36.00 57.00 56.99%

57 69 43

5000 35.40 35.60 35.80 36.00 83 98 112 m/z 71.10 42.38% 140 .... I......... I 182 ' I"' r"'I""I Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190200 210220 Abundance £14795:J;;Pecene, 2.4:dimelhyl- _ 4Q 57

T 83 ■ 35.40 35.60 35.80 36.00 553 in/z 7^710 41.91% 70 112 - —97- 168 I • • ” I > •" I I'' “ I"'' I'' " I 30 40 50 60 70 80 90 100110120 130140 150160170180190 200 210 220 Nsundance #32687: Propanedioic acid, hexyl-, diethyl ester 57- Zte.40-35.60 _35.80_36.60. -------- 70 m/z 112.00 30.85% 5551 83 _112

98 Il 199 217 Tp-nr iSyrMp-J 30 40 50 60 70 80 90 100110120130 140 150160 170 180 190 200 210 220 35.40 35.60 35.80 36.00

23719.D NP091101.M Tue Oct 16 15:14:32 2001 Page 6

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