TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1802\7001.D Vial: 19 Acq On : 19 Apr 2002 5:32 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Undecene, 2,5-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.27 0.38 ug/1 69063 Chrysene-dl2 33.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Undecene, 2,5-dimethyl - 182 C13H26 049622-16-4 32 2 Hexane, 3/- met hyl - 100 C7H16 000589-34-4 27 3 1-Butanol, 2-ethyl- 102 C6H140 000097-95-0 25 4 2,4,4-Tr/imethyl-l-hexene 126 C9H18 051174-12-0 22 Abundance Scan 3075 (33.273 min): 7001 .D (-) m/ z 57.00 100.00% 57 70 1 2 fl 43

5000 83

97 239 256 L 33.00 33.20 33.40 33.60 ' 1 i 1 '

m/z-> T mdh 20 40 1— 60 , lll|li , ili , 80 100 ill

120 129

140 157

160 180 200 207 I

220 I 240 I 260 m/Z 112.10 98.17% Abundance #18488: 2-Undecene, 2,5-dimethyl- 57 69

5000 1 1 i 1 y. ; 1 1 I ' ' 1 1 I ' 33.00 33.20 33.40 33.60 m/z 70.00 85.71% 27 42 3 97 111 126 182 m/z-> . . I ... 1 . i 11 1 1 i ' ' 20 40 4 60 80 100 120 140 160 180 200 220 240 260 Abundance #63421: Hexane, 3-methyl- 43 I 1 1 1 33.00 33.20 33.40 33.60 A 5000 29 57 71 m/z 71.00 85.45%

85 100 i ■ 1 ' 1 i 1 1 i 1 1 I i । । । i i ————।_ । । -i~ । i । । । i । । [ । i — । i i । । । i r-1 r i-! Pi । । mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #63560:1-Butanol, 2-ethyl- - 43 33.00 33.20 33.40 33.60 m/z 43.05 79.83%

5000 70 55 | 31 84 II I. i ' 1 ' 1 i 1 T ! T । i 1 r | I I I I | I I I I | I I I I | I I I I | I I I I | I I I I | I—I—I—I | i 1 I I I I i i i I—r A A AA— m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 33.00 33.20 33.40 33.60

7001 .D GCMS0419.M Mon Apr 22 08:32:43 2002 Page 1

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