Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
NYC-WTC_000043238–000043252Folder label: “GCMS X 4/22/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR12O2\8481. D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.83 2.51 ug/1 491423 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6/91 2 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0-37 3 N-(Trifluoroace'tyl) -0,0',0' '-tris (t 481 C19H34F3NO4Si3 000000-00-0 32 4 N-(Trifluorac.6tyl)-0,0',0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 28 Abundance Scan 1066 (14.829 min): 8481 .D (-) m/z 73.00 100.00%| 73
5000 267 355 ................................ ....................
45 14.40 14.60 14.80 15.00 15.20 । । 108 133154 193 223 . 293 323 1 1 1 1 1 1 । ‘ ■ 1 ■' I 1 H ' y 1 ■ i ■ ■ 1 ■ i 1 m/z 267.00 47.36%| m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 5000 267 J 711 I ' ' 1 1 I ' 1 14.40 14.60 14.80 15.00 15.20 m/ z 355.05 46.93% 207 323 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #57357: Noradrenaline, tetra-TMS 73 .................... . 14.40 14.60 14.80 15.00 15.20 5000 102 355 m/z 356.05 16.24%|
45 147 442 1 1 i mfe-> 50 100 150 200 250 300 350 400 450 [ i । । । | । । । i - i i । i r i i ।—i—r Abundance #58326: N-(Trifluoroacetyl)-O,O',O''-tris(trimethylsilyl)no 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 12.40% 355 5000
45 I 1 । 126147 193 1 i ' 1 1 1 1 1 1 1 1 1 1 265 376 481 .................. | i < i r i । i /..................... I j I I I ] I I I I | I r I | m/z-> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00 15.20
8481.D GCMS0412.M Fri Apr 26 12:47:24 2002 Page 5
NYC-WTC_000043247
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NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044279
Calibration record for GCMS analysis using standard compounds, generated on April 19, 2002, to ensure instrument accuracy.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 1.000
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024997
Laboratory report documenting GCMS analysis of sample AE11309 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023718
Laboratory report of GCMS analysis for sample AE10064 conducted on May 23, 2002, showing surrogate recovery data.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
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NYC-WTC_000043197
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 22 and May 3, 2002.
Filed in the same folder
NYC-WTC_000043198
Partial document page containing fragmented text and a unique record identifier associated with the GCMS testing series from May 2002.
Filed in the same folder
NYC-WTC_000043200
Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE06048 with semi-volatile organic compounds below detection limits from May 3, 2002.
Filed in the same folder
NYC-WTC_000043208
Laboratory report for DEP Box 25 showing GCMS calibration results for sample AE06048 with response factors and MDLs from May 2002.
Filed in the same folder
NYC-WTC_000043212
Laboratory report for DEP Box 25 showing GCMS reference standard analysis of sample AE06048 with measured concentrations from May 3, 2002.
Filed in the same folder