TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR12 02\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Undecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

13.91 0.46 ug/1 66059 1,4-Dichlorobenzene-d4 12.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Undecane 156 C11H24 001120-21-4 2 Tridecane 184 C13H28 000629-50-5 3 Undecane, 4,7-dimethyl- 184 C13H28 017301-32-5 72 4 Hexadecane 226 C16H34 000544-76-3 72 Abundance Scan 966 (13.911 min): 8481 .D (-) m/ z 57.00 100.00% 43 57

5000 71 85 rifi 1 i ' 1 1 ' i 98 156 13.60 13.80 14.00 14.20 113 127 m/z-> 11" ■' । ■ 4 H ...... . 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TWTTTTWTTTTPTTTTTTT ।■I.।.... ।।।. m/ z 43.00 83.82% Abundance #67317: Undecane 43 57

5000 71 13.60 13.80 14.00 14.20 85 m/ Z 71.10 48.64% 27

m/z-> 20 l . 60 70 80 90 100 110 120 130 140 150 160 170 180 190 30 40 50 98 113 156 I | I ! I ! । ! ! ! TIX—, OIJnHtTmunOuO)

Abundance #69020: Tridecane 43 57 1 1 ] I I I 1 ] — 1 — 1 p 1 A/) I /

13.60 13.80 14.00 14.20 5000 71 m/z 41.00 39.84% 85 27 , 99 113 127 141 184 11' ■' ■ i ■ ■1' i TI- ’1121,:11—9—000*EETT018’1 i ■"11" " i r 1 ■' i ■ mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19020: Undecane, 4,7-dimethyl- 43 57 m/z 85.05 30.39%|

5000 71 85

27

m/z-> I 11 ■ ■ ■ ■ i ‘1111' 20 30 40 LU60 70 80 50 i r i - ■ ■ ■ | ■r ■ ■ । ■ 99 113 127 141 TIOHTETTNT_uDuWTIWTTmuug 90 100 110 120 130 140 150 160 170 180 190 AA— / L M / r r ' 'i । । ' i । ' ' ■ । I 13.60 13.80 14.00 14.20

8481.D GCMS0412.M Fri Apr 26 12:47:23 2002 Page 4

NYC-WTC_000043246