GCMS calibration table and instrument parameters, Apr 2002

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Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\APR12 02\8481.D vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Undecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

13.91 0.46 ug/1 66059 1,4-Dichlorobenzene-d4 12.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane 156 C11H24 001120-21-4 /91- 2 Tridecane 184 C13H28 000629-50-5 “78 3 Undecane, 4,7-dimethyl- 184 C13H28 017301-32-5 72 4 Hexadecane 226 C16H34 000544-76-3 72 Abundance Scan 966 (13.911 min): 8481.D(-) m/z 57.00 100.00% 43 57

5000 71 85

98 113 127 156 13.60 13.80 14.00 14.20 — Tp ■ I < I I I I I I I'l I I I I I 111 I I I I I I I I I I I "I I I I I I I I I I I I I I I I I I I I ! m/ Z 43.00 83.82% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #67317: Undecane 43 57

5000 71 13.60 13.80 14.00 14.20 85 m/z 71.10 48.64% 27 .... ...... ...... i । > । । । [ । > । < । i I < i । < i 98 113 156 i 111 i i rr । r i i i । i i i i । i i । । । i rri' j 'i i l i । । । i i i i i i । rrrmpi m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69020: Tridecane 43 57 ' 1 1 I 4T 13.60 13.80 14.00 14.20 71 m/ Z 41.00 39.84% 5000 85 27 ll - TH 99 113 127 1 1 | 1 1 1 1 | 11 1 1 | 1 1 | 1 ‘ 1 141 ' 1 1 1 Vr , I | !! I I | 184 r 1 " i' m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19020: Undecane, 4,7-dimethyl- APAyARv WAvA 43 13.60 13.80 14.00 14.20 57 m/z 85.05 30.39% 5000 71 A 85

27 I 1 | I i ( i । i i । । । r । 99 113 127 141 > । । I I > । '• i ! । । । । i । r। < । । i i r« । i i i i I*i i । । । i i r i । । rrrpri i i |i i i i । i ‘ 1 I I I / 3 .Ar pill I | I i r I | I III | m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 13.60 13.80 14.00 14.20

8481.D GCMS0412.M Wed Apr 17 09:49:08 2002 Page 4

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GCMS calibration table for method GCMS0412, April 2002 · Box DEP Box 27

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