GCMS analysis results for sample AE08762, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8762.D Vial: 24 Acq On : 23 Apr 2002 7:33 am Operator: Sample : gc/ms scan 4/12 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.43 ug/1 75093 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasi xane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 3,4-Dihydrox benzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 64 3 N-(Trifluorpacetyl)-N,O,O ',O1'-tetr 553 C22H42F3NO4Si4 000000-00-0 47 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance 7 Scan 1064 (14.812 min): 8762.D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 | । 154 193 223 , । 323 --------- 1***. m/z 267.00 50.12% m/z-> 50 100 150 200 250 300 350 ‘ 400 ‘ ' 450 ‘ ‘ 500 ' ' 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 .................... / ), , .............. 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 48.01% 323, m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 ....................... ................. . 14.40 14.60 14.80 15.00 15.20 5000 267 m/z 356.05 17.63% 179 356 45 147

m/z—> ' ‘ i 50 ' ' ■ ' i 100 ■ ■ ■ ■ i 150 ■ 209 237, —I 200 250 300 . ................. 4..400 350 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O“-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 13.43% 355 5000

45

miz—> I k • ■ i ■ ■ ‘ ■ i ' ■ 50 100 147 150 193 267 ...... ...................................... 538 .... 1 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

8762.D GCMS0412.M Tue Apr 23 14:24:10 2002 Page 2

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